Children righteousness granules quality standard of.docVIP

 PAGE \* MERGEFORMAT 8 Children righteousness granules quality standard of [Abstract] Objective: To establish quality standards for particulate righteous children. Methods: TLC-scanning of Astragalus Astragaloside content. Results: astragaloside in the range of 1.005 ~ 6.030 μ g has good linear relationship, r = 0.999, average recovery was 97.02%, RSD = 1.80%. Conclusion: The quality standards can effectively control the quality of children uprightness particles. [Keywords:] Children righteousness quality standards for particulate TLC Astragaloside Children righteousness particles from Astragalus, psoralen, etc. 5 Herbs, has a Bufei spleen, kidney strengthening the foundation of the effect, for all the physical weakness, sick children with recurrent respiratory tract infections. To control its quality to ensure its efficacy, using TLC scanning method Astragalus contains astragaloside to assay, reported as follows. An experimental material CS  9301 dual-wavelength scanner (Shimadzu, Japan), astragaloside Chemical Reference (by the Chinese pharmaceutical and biological products to offer Lot: 0781  9906, specification: for determination purposes), and the reagents were HPLC pure and AR. 2 Determination 2.1 Agent for chloroform - methanol - butanol - water (2:1:4:1) 10 ℃ below the lower place overnight. 2.2 Reference Standards and test items for the preparation of solution 2.2.1 Preparation of reference substance solution precision that an appropriate reference substance obtained Astragaloside, Canada is made for every 1 mL methanol containing 20 μ g of the solution, that is, too. 2.2.2 Preparation for the test product solution to take this product under the load difference of contents, mixing, take about 2.5g, precision, said determined set Soxhlet extractor, add methanol 80 mL, reflux extraction 4 h, extract evaporated, add water, 20 mL, water saturated ether extracted three times, each time 20 mL, discarded to the ether solution with water satur