Determination by HPLC Bushenqiangshen Capsule icariin.docVIP

 PAGE \* MERGEFORMAT 7 Determination by HPLC Bushenqiangshen Capsule icariin [Abstract] Bushenqiangshen capsules established method for the determination. Methods HPLC determination Bushenqiangshen Icariin capsule. The results of icariin in the range of 0.2052 ~ 1.0260μ g a good linear relationship, with an average recovery of 98.39%, RSD of 1.93% (n = 9). Conclusion The method is highly specific, high sensitivity, good reproducibility can be used to control Bushenqiangshen capsules. [Keywords:] HPLC Bushenqiangshen capsules Icariin [Abstract] Objective To establish a method for determination for icariin in Bushenqiangshen Capsules. Methods The contents of icariin were determined by HPLC. Results Icariin showed a good linear relationship at the range of 0.2076 ~ 1.0380μ g. The average recovery was 98.39%, and RSD was 1.93% (n = 9). Conclusion The method is sensitive, with strong specificity and reproducibility, and can be used for quality control of Bushenqiangshen Capsule. [Keywords:] bushenqiangshen capsule; icariin; HPLC Bushenqiangshen capsule from epimedium, Rosa laevigata, Dodder, Ligustrum lucidum, Woodwardia Gomi medicinal composition, income contained in the ‘Ministry of Health standards by the set prescription drug agents’ fourth book, with kidney physical effect. For the treatment of lumbar acid-foot soft, dizziness, tinnitus, vertigo palpitations, impotence and other diseases spermatorrhea. The quality standards of the preparation is too simple, only its characters were described, there is no determination of the method, can not effectively control the quality of the preparation. In order to improve quality standards, the present study, HPLC method for Epimedium icariin in the determination of [1]   1 instruments and reagents 1.1 Instrument Waters HPLC: 1525 pump, 2996 UV detector, 1500 column temperature boxes, 717 Autosampler; AG-135 electronic balance [Mettler - Toledo (Shanghai) Co., Ltd.]. 1.2 reagent icariin reference substance (