Guanxin Danshen Pill by TLC of.docVIP

 PAGE \* MERGEFORMAT 9 Guanxin Danshen Pill by TLC of 【Abstract】 Objective In this paper, thin-layer chromatography for identification of Guanxin Danshen Dropping Pill determined. Methods According to the characteristics of the composition Guanxin Danshen Dropping Pill, choose the appropriate developing agent systems for qualitative identification. Results and Conclusion The method is simple, quick, reproducible, they could effectively control the quality of the preparation. Keywords: thin-layer chromatography; Guanxin Danshen Dropping Pill; 37 saponins R1; tanshinone Ⅱ A; Sal B Guanxin Danshen Dropping Pill is Salvia, 37, descending the composition of sesame oil compound preparation in clinical chest tightness caused heartache for Qi stagnation blood stasis, Zheng Jian chest tightness, chest pain, shortness of breath, palpitations, coronary heart disease colic embolism significant effect. To effectively control the product quality, this paper thin-layer chromatography carried out more than a qualitative identification of the shamisen, traditional Chinese medicine. A reagent of the test drug Tanshinone Ⅱ A reference substance, Danshen control medicine, Sal B reference substance, dalbergia control medicines, 37 control medicine, 37 saponins R1 reference substance (China provided medicines and biological products); Coronary Danshen Pill Samples (batch20070503, medium-fat sharp Pharmaceutical Industrial Group Industry Co., Ltd.); silica gel G plates (Qingdao Marine Chemical Plant); polyamide film (Taizhou Luqiao tetracarboxylic Biochemical Plastics Factory); Methanol and other reagents were analytical pure. 2 TLC To take this product 1g, heating water, 20ml, stirring allows the dissolved and transferred to the separatory funnel, add ethyl ether extraction two times, respectively, 20ml, 10ml, combined ether extract, Hui dry, add methanol 1ml allows the dissolved residue, as for the test product solutio