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High Performance Liquid Chromatography Chuanping pills Scopolamine content
PAGE \* MERGEFORMAT 9
High Performance Liquid Chromatography Chuanping pills Scopolamine content
Authors: Xiao-Yan Li, Feng, the WU Yan-Hong, ZHU Sheng-Shan, Huo Wuzhen
[Abstract] Objective To determine the alkali content Chuanping Pill scopoletin high-performance liquid chromatography. Methods ZORBAX SB-C18 (4.6 mm * 250 mm, 5 μ m) as column, methanol -0.001 mol * L-1 phosphate (70:30) (mobile phase containing 0.02 mol * L-1 sodium dodecyl sulfate sodium) as the mobile phase, detection wavelength: 216 nm, flow rate: 1.0 ml * min-1, external standard method. The results of scopolamine 0.028 5 ~ 0.285 μ g in the context of a linear relationship between recovery was 98.86% (n = 6), RSD 2.54%. Conclusion This method is simple, accurate, reproducible and can be used for asthma scopoletin alkali content measured flat pills.
[Keywords:] high-performance liquid chromatography Chuanping pills Scopolamine
Chuan-ping pills from ephedra, Datura metel and other traditional Chinese medicine composed of Chinese herbal compound preparation. The main chemical constituents of Datura metel in which scopolamine, a significant hub of inhibition, anesthetic effect, typical doses will be able to eliminate emotional and engender weariness into a dreamless sleep state, resulting in ‘forgetfulness’ embolism, severe drowsiness , coma and finally died of respiratory center inhibition or paralysis, respiratory and circulatory failure. Fang, although the quantity Yangjinhua small proportion of prescriptions, in order that the compound preparation of medication safety, the research group of the compound preparation of trace levels of scopolamine for monitoring the safe use of the drug to provide data for reference.
An instrument and reagent
1.1 Instrument
Agilent1100 series of high-performance liquid chromatography (G1311A quaternary pump, G1313A autosampler, G1314A-VWD detector); Column: ZORBAX SB-C18 (4.6 mm * 250 mm, 5 μ m), SN: USCL017850, BP211D e analytical balance (Sartori
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