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High Performance Liquid Chromatography claw capsule compound ferulic acid
PAGE \* MERGEFORMAT 8
High Performance Liquid Chromatography claw capsule compound ferulic acid
Author: Zhou Ying, Li Shuqing, Liu Yonggang
[Abstract] Objective To establish a claw capsule compound ferulic acid by HPLC. Methods Diamonsil-C18 column (5 μ m, 250 mm * 4.6 mm); mobile phase: methanol - water - glacial acetic acid (30:70:1); detection wavelength: 320 nm; flow rate: 1.0 ml / min. The results of ferulic acid in the 8 ~ 80 μ g / ml range, the peak area and concentration showed a good linear relationship, r = 0.9998, average recovery was 99.56%. Conclusion The method is simple, rapid, sensitive, accurate, and can be used as a method for determination of the preparation.
[Keywords:] compound claw capsules; ferulic acid; high-performance liquid chromatography
[Abstract] Objective To establish a determination method of the content of ferulaic acid in Yangjiao capsules. Methods The content of ferulaic acid in Yangjiao capsules was determined by HPLC and Diamonsil-C18 column (250 mm * 4.6 mm, 5μ m) was used. The mobile phase was a mixture of methanol-water-glacial acetic acid (30:70:1), column temperature was 25 ℃ , the flow rate was 1 ml / min and the detection wavel ength was 320 nm. Results The calibration curve of ferulaic acid was linear over the range of 8 ~ 80μ g/ml.The average recovery rate was 99.56%. Conclusion The method is simple, fast, sensitive and can be used to assess the quality of Fufang Yangjiao capsules.
[Keywords:] Fufang Yangjiao capsule; ferulaic acid; high performance liquid chromatography
Claw capsule compound is contained in the original income ‘drug regularized standard’ No. 4, prescription by the cyclone, Chuanxiong, Angelica, the system Chuanwu 4 Herbs, has a Pinggan, analgesic. For migraine headache, vascular headache, tension headache, but also can be used for neuralgia. Jun prescription drug claw nitrogen content has been provided, while Robinson Chuanxiong Quewu determination of drug targets to improve drug quality sta
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