Near-infrared spectroscopypartial least-squares method for rapid determination of star anise in the shikimic acid content in.doc

 PAGE \* MERGEFORMAT 13 Near-infrared spectroscopypartial least-squares method for rapid determination of star anise in the shikimic acid content in Authors: Fan Ming-yin, Meng Fan, Wang Di, Wang natural, Yang, TENG Li-rong, LIN Feng [Abstract] Objective partial least squares (PLS) To determine the star anise in the shikimic acid content in near-infrared spectroscopy quantitative analysis model. Methods Using a variety of spectral pretreatment, respectively star anise powder near-infrared spectra of the sample pretreatment, using the spectral pretreatment, respectively, after the establishment of quantitative analysis models, the model selected the optimal number of main factors to optimize. Comparing the results of each model through the internal cross-validation root mean square error (RMSECV) and the cross-validation predicted values with the experimental measured values of the correlation coefficient between the (Rv), the external root mean square error (RMSEP), select the optimal model. Conclusion The results show good robustness of quantitative analysis models and forecasting, high precision, quantitative analysis of the effective components of Chinese medicine has great application prospect. [Keywords:] Star Anise near-infrared spectroscopy PLS shikimic acid Star Anise Star Anise for Magnoliaceae Illicium verum Hook f. dry ripe fruit, produced in southern China and Vietnam, is an important ‘Medicinal and Edible’ economic tree species for our specialty spice and herbal medicine. Star Anise generally contain shikimic acid, is a rich source of shikimic acid. Studies have shown that shikimic acid has good anti-inflammatory, analgesic, and the role of inhibiting platelet aggregation, is effective against the deadly H5N1 strain of bird flu drug ‘Tamiflu’ synthetic intermediates [1,2], with a broad development values and application prospects. Near-infrared spectroscopy in the wavelength range 780 ~ 2 500 nm, organic compounds are absorbed in the area. C