Of proprietary Chinese medicines by atomic absorption spectrophotometry of magnesium manganese copper zinc and iron content determination.docVIP
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Of proprietary Chinese medicines by atomic absorption spectrophotometry of magnesium manganese copper zinc and iron content determination
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Of proprietary Chinese medicines by atomic absorption spectrophotometry of magnesium manganese copper zinc and iron content determination
[Keywords:] FAAS; Chinese medicine; metal elements
0 Introduction The efficacy of Chinese medicine is not only concerned with one of the organic ingredients, but also with trace elements, macro elements and functional relevance [1-2]. We use flame atomic absorption spectrophotometric determination of 10 kinds of the brain such as plug-pass in Chinese traditional medicines manganese, magnesium, iron, zinc and copper content of five kinds of elements to explore the Chinese traditional medicines of trace elements and macro elements and treatment of cerebral vascular disease relationship.
1 Materials and methods
1.1 Materials brain Sai Tong (Tonghua Maoxiang Pharmaceutical Co., Ltd.); strong Gastrodia Eucommia Pills (Shandong Zhongtian Pharmaceutical Co., Ltd.); Tongsaimai tablets (Jiangsu Southern Star Pharmaceutical Co., Ltd.); Tongmaining Granule (Shanghai West Pharmaceutical Co., Ltd.); Maitong (Guangzhou Pulse Technologies Co., Ltd.); compound Ginkgo biloba capsules, large rolling Dan (39 Huangshi Pharmaceutical Factory); Zhongfenghuichun tablets (Henan Yuzhou Medicine King Pharmaceuticals Co., Ltd.) ; Xiaoshuan Capsules (Golden Square, Xi’an, Shaanxi Hi-Tech Pharmaceutical Company); to Austria zhinbiticose (Chengdu Diao Group); WFX Ⅱ -type atomic absorption spectrophotometer (Shanghai Instrument Factory); HNO3, HClO4 are made Top-grade pure.
1.2 Methods to take 10 pills each pill, tablet taken 10 by throwing pieces mixing, each sample parallel to obtain two copies, each 1.0 000 g, placed in 25 mL conical flask, add HNO3 10 mL, sealed overnight ; the next day was added HNO3 10 mL, HClO4 5 mL, electric board at the slow heating, when the remaining approximately 2 mL were added again when the HNO3 20 mL, HClO4 5 mL, to continue to digest, to the solution was colorless and transparent in recent dr
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