Phenolic resin laminate substrate to characterize the products of vacuum pyrolysis_0.doc

 PAGE \* MERGEFORMAT 13 Phenolic resin laminate substrate to characterize the products of vacuum pyrolysis Of: * Licheng Long Xu Xiao Qiu Keqiang Wu Wenbiao group [Abstract] The pyrolysis oven temperature program of the phenolic resin reactor vacuum pyrolysis laminate substrates, by elemental analysis, Fourier transform infrared (FT-IR analysis and gas chromatography - mass spectrometry (GC-MS analysis of raw materials and Oil products were characterized. Research shows that pyrolysis oil is mainly the supernatant are more vulnerable to water-soluble substances, such as phenol, cresol, xylenol, carbohydrate, hydantoin type, morpholine class pyran compounds, ketones and pyridine, and lower precipitation are mainly water insoluble or hardly soluble substances, such as major phenolic substituents (substituent carbon atomsgt; = 2, aryl phosphate esters, fatty acid esters and nitrile compounds. Among them, the melamine in the upper and lower precipitation in the serum has a higher content. [Keywords:] laminate substrates, vacuum pyrolysis, phenolic resin, characterization ProductAbstract Vacuum pyrolysis of phenolic resin laminate substrate in temperature-programmed furnace reactor was studied.The sample and product oils were characterized by elemental analysis, Fourier transform infrared (FT-IR) analysis and gas chromatography-mass spectrometry (GC-MS). Analytical results showed that the upper clear liquid of pyrolysis oils was mainly consisted of water-soluble substances, such as phenol, cresol, xylenol, sugars, hydantoins, morpholines, pyranones and pyridine derivatives compounds, etc., while the lower sediment was mainly insoluble or hardly water-soluble substances, such as the big substituent phenolics (the number of substituent carbon atoms of which is greater than or equal to 2), aryl phosphate esters, fatty acid esters and nitrile compounds, and so on.Both of the upper clear liquid and lower sediment have a higher content of melamines. Keyword