Poria ultrafine powder and the volatile constituents of ordinary.doc

 PAGE \* MERGEFORMAT 9 Poria ultrafine powder and the volatile constituents of ordinary Author: Liao Chuan, Yang Nai-Jia, Liu Jianhua, Huang Jian City, Ding Lina, Yuan Yueling [Abstract] Objective To study the volatile components Poria. Methods using organic solvents - Poria volatile components extracted by steam distillation, using GC / MS for separation and determination, combined with computer retrieval technology structure elucidation of isolated compounds, the application chromatographic peak area normalization method to calculate the relative percentage content of each component. Results Poria ultrafine isolated 131 components were identified 67 chemical constituents, accounting for 51.145 percent of the total volatile oil; Poria-powder 103 isolated components, Kam out of 61 chemical components, accounting for 59.223 percent total volatile oil. Poria two kinds of volatile oil components in powder, contains 57 kinds of the same composition, in which the highest concentrations found were α -Cypress ol (Poria ultrafine 7.936%), anti-nerolidol (Poria-powder 8.657%). Conclusion first reported the use of simple organic solvents - Poria ultrafine powder extracted by steam distillation of volatile components, and with the Poria-powder together qualitative and quantitative comparative study. [Keywords:] Poria ultrafine; Poria-powder; organic solvents - steam distillation; volatile oil; gas chromatography - mass spectrometry Abstract: ObjectiveTo study the chemical constituents of the volatile oil from Poria cocos.MethodsThe chemical compositions of the volatile oil of the plants which were obtained by organic-steam distillation with hexane were analyzed by GC-MS. The constituents were identified by their mass spectra . The relative percentage of the oil constituents was calculated from the GC peak areas. ResultsOne hundred and thirty-one kinds of chemical constituents in micro-milling of Poria cocos were separated, of which sixty-seven compounds representing 5