Qingnao Jiangyapian Quality Standards.doc

 PAGE \* MERGEFORMAT 18 Qingnao Jiangyapian Quality Standards Authors: Zeng Hui-fang, Cai can, Huang their, Yao Hui, Hou Shao-Zhen, Peng Shaozhong 【Abstract】 Objective To establish a clear cerebral blood pressure tablets quality control standards. Thin Layer Chromatography preparations angelica, cassia seed; using high performance liquid chromatography preparation of baicalin. The results angelica, cassia seed thin spots atlas clear, blank and without interference; baicalin in the range of 0.076 ~ 1.52 mg a linear regression equation Y = 52.585X-0.294 2, r = 0.999 9, the average recovery was 100.36 %. RSD = 1.67% (n = 9). Conclusion The established method is simple, accurate, fast, stable, reliable and can be used as the preparation of quality control standards. Keywords: Qingnao antihypertensive tablets; thin-layer chromatography; quality standards; baicalin Abstract: ObjectiveTo establish the quality standard of Qingnao Jiangya Tablet.MethodsTo identify Radix Angelica Sinensis and Semen Clssiae by TLC. Determine baicalin by HPLC.ResultsRadix Angelica Sinensis and Semen Clssiae had a sharp chromatogram by TLC. The standard curve of baicalin was Y = 52.585 X-0.294 2, r = 0.999 9, linear range was 0.076 ~ 1.52 mg, average recovery rate of baicalin was 100.36%, RSD was 1.67%. ConclusionThe method is simple, accurate and can be used for the quality control of the granules. Keywords:: Qingnao Jiangya; Tablet; TLC; Quality standard; Baicalin Qingnao buck the standard closed-chip is contained in the “Chinese Pharmacopoeia” 2005 edition, prescription from the skullcap, angelica, cassia seed composed of 13 Chinese herbal medicines, has Pinggan Qian Yang, Qing brain buck effect. For liver yang, high blood pressure, dizziness, dizziness, insomnia, forgetfulness and so on. Current “Chinese Pharmacopoeia” standards are only recorded in the other side of angelica and cassia seed for TLC, and have not been content determination [