Quality Standard of Tianqi.doc

 PAGE \* MERGEFORMAT 10 Quality Standard of Tianqi [Abstract] Objective To establish quality standards for particles Tianqi. Methods of prescription in the TLC method for qualitative identification of Panax notoginseng by HPLC method of ginsenoside Rg1 on the preparation and quantitative determination of notoginsenoside R1. Results in TLC to identify the detection Panax ginseng saponin Rg1 in 0.628 ~ 5.652 μg (r = 0.999 8), R1 in notoginsenoside 0.155 ~ 1.395 μg (r = 0.999 8) was linear within the relationship, the average recovery was 99.24 % (RSD = 0.84%) and 99.14% (RSD = 1.13%). Conclusion The method is simple, accurate, reproducible, high precision, can be used as for the quality control methods. [Keywords:] Tianqi particles, thin layer chromatography, ginsenoside Rg1, Notoginsenoside R1, high performance liquid chromatography Abstract: Objective To establish the quality standard for Tianqi Granule. Methods Radix Notoginseng in Tianqi Granule was identified by TLC. The ginsenoside Rg1 and notoginsenoide R1 in Tianqi were determined by HPLC. Result Radix Notoginseng could be identified by TLC. The linear ranges of ginsenoside Rg1 and notoginsenoide R1 were at 0.628 ~ 5.652 μg (r = 0.999 8) and 0.155 ~ 1.395 μg (r = 0.999 8), respectively. The average recoveries were 99.24% (RSD = 0.84%) and 99.14% (RSD = 1.13% ). Conclusion The method is simple, accurate and with good reproducibility and high precision, and can be used for quality control of Tianqi Granule. Keywords:: Tianqi Granule, TLC, ginsenoside Rg1, notoginsenoide R1, HPLC Panax pseudo-ginseng particles is mainly made of raw materials, with blood and pain, stasis of the new health role. Panax ginseng saponins containing mainly Rb1, Rg1, Re and R1 notoginsenoside more than 20 kinds of saponins, including ginseng ginsenoside Rb1, Rg1 and Notoginsenoside R1 is the highest content of 3 components, Panax notoginseng R1 is the characteristic components [1]. The trial of the drug product wer