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Quality Standards Bazhen Yimu Pills Research
PAGE \* MERGEFORMAT 18
Quality Standards Bazhen Yimu Pills Research
Author: Tian Shuang-yan, Yuanzhi Fang, Chen Weiping, Zhang Tong
[Abstract] Objective To establish Bazhen Yimu Pills quality control standards. Methods using thin-layer chromatography Bazhen Yimu Pills prescription Motherwort, Codonopsis, Poria, licorice root, white peony root (Jiuchao), etc. Chinese medicine for qualitative identification; using high performance liquid chromatography in Bazhen Yimu Pills Stachydrine hydrochloride content. Chromatographic conditions: Spherisorb SCX (150 mm * 4.6 mm) column, sodium dihydrogen phosphate solution (pH3.5) as mobile phase, detection wavelength of 194 nm, flow rate of 1.0 ml * min-1, the column temperature at room temperature, The injection volume of 20 μ l. Results Motherwort, Codonopsis, Poria, licorice root, white peony root (Jiuchao) using the appropriate method of TLC, TLC control after the commencement of medicinal herbs have shown that the specificity of the same spots, separation effect is good. Stachydrine hydrochloride concentration in the 1.104 ~ 8.832 μ g * ml-1 and the peak area within the framework of a good linear relationship, regression equation Y = 533 369X 60 637, the correlation coefficient r = 0.996 5 (n = 6). The average recovery was 98.38%, RSD 0.24%. Conclusion The method is accurate, reliable, specific, can be used to Bazhen Yimu Pills quality control.
[Keywords:] thin-layer chromatography; high-performance liquid chromatography; hydrochloride Stachydrine; Bazhen Yimu Pills
Abstract: ObjectiveTo establish a quality standard of Bazhenyimu Concentrated Pill. MethodsTraditional Chinese medicine in prescription such as herba Leonuri, Poria, Radix Paeoniae Alba were identified by a series of TLC methods. The content of stachydrine hydrochloride in Bazhenyimu Concentrated Pill was determined by HPLC method . Spherisorb SCX (150 mm * 4.6 mm) column was used, the mobile phase was sodium dihydrogen phosphate buffer solution (pH3
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