Catalyst Composition and Content Effects on the Synthesis of Single-Walled Carbon Nanotubes by Arc Discharge英文文献资料.docVIP

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Catalyst Composition and Content Effects on the Synthesis of Single-Walled Carbon Nanotubes by Arc Discharge英文文献资料.doc

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Catalyst Composition and Content Effects on the Synthesis of Single-Walled Carbon Nanotubes by Arc Discharge英文文献资料

HindawiPublishingCorporation JournalofNanomaterials Volume2007,ArticleID84540,4pages doi:10.1155/2007/84540 ResearchArticle CatalystCompositionandContentEffectsontheSynthesisof Single-WalledCarbonNanotubesbyArcDischarge TingkaiZhao,1,2QinghuTang,3YongningLiu,1ChangchunZhu,2andXiangZhao4 1 2 3 4 StateKeyLaboratoryforMechanicalBehaviorofMaterials,Xi’anJiaotongUniversity,Xi’an710049,China SchoolofElectronicsandInformationEngineering,Xi’anJiaotongUniversity,Xi’an710049,China SchoolofEnergyandPowerEngineering,Xi’anJiaotongUniversity,Xi’an710049,China SchoolofScience,Xi’anJiaotongUniversity,Xi’an710049,China Received15January2007;Accepted16March2007 RecommendedbyRakeshK.Joshi Single-walledcarbonnanotubes(SWCNTs)werepreparedbyamodi?edarcdischargingfurnaceusingFe-Ni-Mgpowdersas ? catalystat600 C.Thee?ectsofcatalystcompositionandcontentontheproductionrateandpurityofSWCNTsareinvestigated inthispaper. WhentheFe-Ni-Mgcatalystcompositionis2:1:2wt% andthecatalystcontentis5wt%, theexperimental resultsindicatethattheproductionofSWCNTsis12gramsperhour,andthepurityanddiameterofSWCNTsare70%and1.22 ～1.38nm,respectively.Theresultsindicatethatthecooperativefunctionofcatalystcompositionandcontentplaysanimportant roleintheproductionofSWCNTs.TheaimofthisworkistocontroltheproductionprocessofSWCNTse?ciently. Copyright?2007TingkaiZhaoetal.ThisisanopenaccessarticledistributedundertheCreativeCommonsAttributionLicense, whichpermitsunrestricteduse,distribution,andreproductioninanymedium,providedtheoriginalworkisproperlycited. 1. INTRODUCTION productionofSWCNTsundercertainconditions.According topreviousliteratures[6,7],Fe?Ni?Mgpowderascat- alystisoneofthemoree?cientcatalyststoprepareSWC- NTsbyarcdischargingfurnaceatcontrolledtemperatureon largescaleandhighpurityatpresent.Thee?ectoftempera- tureontheformationofSWCNTshasbeenstudiedindetail [6].However,thee?ectsofcatalystcompositionandcontent onthegrowthofSWCNTsarenotwellinvestigatedinprevi- ouspaper.Therefore,itisnecessarytocarryoutthisre