Coordination Polymer Synthesis, Spectral Characterization and Thermal Behaviour of Starch-Urea Based Biodegradable Polymer and Its Polymer Metal Complexes英文文献资料.docVIP

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Coordination Polymer Synthesis, Spectral Characterization and Thermal Behaviour of Starch-Urea Based Biodegradable Polymer and Its Polymer Metal Complexes英文文献资料.doc

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Coordination Polymer Synthesis, Spectral Characterization and Thermal Behaviour of Starch-Urea Based Biodegradable Polymer and Its Polymer Metal Complexes英文文献资料

HindawiPublishingCorporation BioinorganicChemistryandApplications Volume2010,ArticleID848130,8pages doi:10.1155/2010/848130 ResearchArticle CoordinationPolymer:Synthesis,SpectralCharacterizationand ThermalBehaviourofStarch-UreaBasedBiodegradablePolymer andItsPolymerMetalComplexes AshrafMalik, ShadmaParveen, TansirAhamad, SaadM.Alshehri, PrabalKumarSingh, 1 1 2 2 1 andNahidNishat 2 1 2 MaterialsResearchlaboratory,DepartmentofChemistry,JamiaMilliaIslamia,NewDelhi110025,India DepartmentofChemistry,KingSaudUniversity,Riyadh1145,SaudiArabia CorrespondenceshouldbeaddressedtoNahidNishat,nishatnchem08@ Received18February2009;Revised19July2009;Accepted30March2010 AcademicEditor:DimitrisKessisoglou Copyright?2010AshrafMaliketal.ThisisanopenaccessarticledistributedundertheCreativeCommonsAttributionLicense, whichpermitsunrestricteduse,distribution,andreproductioninanymedium,providedtheoriginalworkisproperlycited. Astarch-urea-basedbiodegradablecoordinationpolymermodi?edbytransitionmetalMn(II),Co(II),Ni(II),Cu(II),andZn(II) waspreparedbypolycondensationofstarchandurea.AllthesynthesizedpolymericcompoundswerecharacterizedbyFourier 1 13 transform-infraredspectroscopy(FT-IR), H-NMRspectroscopy, C-NMRspectroscopy,UV-visiblespectra,magneticmoment measurements,di?erentialscanningcalorimeter(DSC),andthermogravimetricanalysis(TGA).Theresultsofelectronicspectra andmagneticmomentmeasurementsindicatethatMn(II),Co(II),andNi(II)complexesshowoctahedralgeometry,whileCu(II) andZn(II)complexesshowsquareplanarandtetrahedralgeometry,respectively.Thethermogravimetricanalysisrevealedthatall thepolymericmetalcomplexesaremorethermallystablethantheparentalligand.Inaddition,biodegradablestudiesofallthe polymericcompoundswerealsocarriedoutthroughASTMstandardsofbiodegradablepolymersbyCO2evolutionmethod. 1.Introduction (e.g.,polylacticacid).Chemicallysynthesizedpolymersfrom monomers obtained commercially by ch