29种有机磷农药向卷烟主流烟气粒相物和烟蒂中的转移率.pdfVIP

烟草科技ITobacco Science Technology 烟草化学ITobacco Chemistry 2010 年第 7 期(总第 276 期) 29 种有机磷农药向卷烟直流烟气粒相物和烟蒂中的转移率 张烘非1. 胡清踊1 ，幽纲崎1 ，边照阳1 ，正 常2 1.国家烟草质量f 监督检验中心，郑州高新技术产业开发区枫杨街2 号 450001 2. 深刻l 卷烟厂，广东省深圳市保安区龙华街道清湖工业园 518109 关键调:卷烟;吃相色谐 m 质增;有机磷农药;.i.流烟气;烟蒂;转移卒 摘票:考寨了添加在烟直生中的 29 种有机磷农药向卷烟主流烟气粒相物和烟蒂的转移情况。结果表明: 这些农药向卷烟主流烟气粒相物中的平均转移率为 0-6.39岛，相对标准偏差为 8.0%-189岛，烟蒂的平 均截留率为 0.3% -15% ，相对标准偏差为 6.5% -21%0 中朋分3障碍:S4 81 + • 8 ; TS4 11 文献标识码 :B 文尊重捕号: 1002 -0861 (2010)07 叩 0039 -04 Transfer or 29 Organophosphorus Pesticides in Cut Tobacco to Particulate Matter in Mainstream Cigarette Smoke and Cigarette Butt ZHANG HONG-FEI( 1) , HU QING-YUAN (1) , TANG GANG翩LING( 1) , BTAN ZHAO-YANG( 1) , and WANG FANG(2) 1. China National Tobacco Quality Supervision Test Center , Zhengzhou 450001 , China 2. Shenzhen Cigarette Factory , Shenzhen 518109 , Guangdong , China Keywords: Cigarette; Gas chrornatography/rnass spectrornetry; Organophosphorus pesticide; Mainstrearn cigarette srnoke (MCS); Cigarette butt; Transfer rate Abstract: 29 organophosphorus pesticides were added into the test cigarettes , the transfer rates of these pesticides to the particulate rnatter (PM) in rnainstrearn cigarette srnoke and cigarette butts were deterrnined with gas chrornatography/rnass spectrornetry. The results indicated that the average transfer rates to PM in MCS was 0 -6. 3 % with the relative standard deviations CRSDs) of 8. 0% -189毛 and the average retention rate of cigarette butts was 0.39奋斗5% wíth the RSDs of 6. 5% -21 %. 自前，有机磷农药向卷烟主流炯气和!烟烟带的转移 1 材料句方法 率研究[口1川俐斗刊1 1. 1 仪器与试剂 采用加栋怯研究了有机磷农药向若潜寄烟才主三流炯气和娴蒂 的转移率，旨在为卷炯减害和危害性评价提供参考。 ASE200 加速榕剂萃取仪(美国 Díonex 公司) ，配 到 rnL 不