空气_乙炔火焰原子吸收光谱法测定头发中钙元素含量的方法及研究.pdfVIP

22 4 Vo .l 22, N o. 4 200 8 4 Ch em ica l Indu s try Tmi e s Apr. 4. 200 8 - 徐学笛 (, 430074) - (AAS), , , 1. 5% , , 3+ (- - ) La , . , , R SD 0. 5% , 97. 0% Study on D eterm in at ion of th e C onten t of C a lcium in H a ir by A tom ic Ab srp t ion Sp ectrom etry w ith A ir - Acety lene F lam Xu Xuedi ( Fa ulty ofM aterials S ien e and Chem i alEngineering, Ch inaUniversity ofGeos ien es, HubeiWuhan 430074) Ab str act Determ in ing of the on tent of, al ium in hair by atom i absrption spe trometry w ith air- a etylene flam, expermi ental ondition, intereren es and its elmi inatedm ethod, and the added volume ofhydro h lori a id were stud ied. When the a idity ofdeterm ined solution was under 1. 5% , in the presen e of lanthanum oxide used as relea2 sing agen,t the resu lt ob tainedwas stab le and reliable. The sampleswere de omposed by omposited a ids, and inter2 feren e of oexist omponentswas effe tiviely elmi inated using the omposited inhibitors of ( as orb i a id + lan tha2 num + niob ium ). Thismethodwas smi ple, rap id and had good pre ision and a ura y. The relative standard deriva2 tion was 0. 5% . The re overy ratewas 97. 0% . K eyw ord s Flame Atom i Absorption Spe trophotometry al ium determ ination FAAS [ 5~ 7] , , L. Pszon i ki [ 1] ZnFeCa , , , , [2 ] , , , , , ,