Er掺杂纳米ZnO的制备及紫外光催化降解罗丹明B_戚丽.pdfVIP

34 8 Vol.34 No.8 2015 8 ELECTRONIC COMPONENTS AND MATERIALS Aug. 2015 Er ZnO B Er ZnO Er-ZnO XRDFT-IR SEM Er-ZnO Er-ZnO B Er-ZnO 16~30 nm 700 4.5 hEr 0.2%Er-ZnO 3 h0.02 g·L–1 B pH≈9 73.7% Er ZnO B doi: 10.14106/ki.1001-2028.2015.08.004 X131.2 A 100108-0013-05 Preparation of Er-doped ZnO nanoparticles and its photodegradation on Rhodamine B under ultraviolet QI Li, GUO Dazheng, ZOU Ruyi, ZHU Zhenzhen (Shangrao Normal University, Shangrao 334001, Jiangxi Province, China) Abstract: Er-doped ZnO nanoparticles (Er-ZnO) were synthesized by ultrasonic assisted method. Their crystal structures were characterized by XRD, FT-IR and SEM, and their photocatalytic activity toward the degradation of Rhodamine B was studied. The results show that the Er-ZnO crystal particles possess hexagonal wurtzite structures with a particle size of 16–30 nm, which self-assemble into bigger spindle porous particles. Furthermore, the 0.2% (mass fraction) Er-doped ZnO calcinated at 700 for 4.5 h exhibits the highest photocatalytic ability, and the degradation rate of sample to Rhodamine B solution (0.02 g•L–1 , the initial pH is 9) reaches 73.7% under UV irradiation for 3 h at room temperature. Key words: ultrasonic assisted synthesis; Er; ZnO; Rhodamine B; photocatalytic; calcination; degradation rate B(Rhodamine B) InO ZnSSrTiO 3 3 [1]TiO 2 ZnO