微波消解-石墨炉原子吸收光谱法对乳制品中铅质量分数的测定.pdfVIP

wvcw．cIlirla蛐。net 中国乳品工业 z卿g)，@163．com 微波消解一石墨炉原子吸收光谱法对乳制品中铅质量分 数的测定 王曹，陈伟，熊砍，张漓平，代静 (重庆天友乳业股份有限公司技术中心，重庆400060) 摘要：采用微波消解技术处理样品，减少了被测元素的损失。对石墨炉的灰化温度、原子化温度和基体改性剂等条件进行了优化，筛 标准偏差为O．81％-3．18％。本方法具有检出限低、简便、快速、试剂用量少、干扰少等优点，适合用于分析乳和乳制品中铅的质量分数。 关键词：微波消解；石墨炉原子吸收光谱仪；乳帝】品；铅；测定 中圈分类号：TS252．7 文献标识码：A 文章编号：1001-2230(2014)04-0059-03 milkandmilk microwavefa- Leaddeterminationin through products digestion atomic cilitated furnace graphite absorptionspectrometry WANG Wei，XIONGXin，ZHANG Rong，CHEN Qillg—ping，DAIJing of Industrial (Center 400060，China) Technology,TianyouDairy aCo．Ltd．，Chongqing were microwave toreducethelossofthetestedelement．Theconditionsof treated Abstract：Samplesby digestiontechnique optimal leaddeterminationfurnaceatomic wereobtained intensive ofvarious f-u!-n盅ce absorption through screemg bygraphite spectrometry graphite andmatrixmodification the methoddetection conditions，the limitwas ashingtemperatures，atomizationtemperatures agents．Underoptimal 0．21 of WaS85．2％～101．3％andthereladvestandarddeviationWaSO．81％--3．18％．Thismethodfeatureslowdetection recovery I止g／L．rate and issuitableforthe of inmilk interference，etc．and leadcontent and limit，simplerapidoperation。lessreagentconsumption，less maiym milk products． words：microwave flllT硷Ceatomic Key digestion；graphite