化工原理实验——精馏综合实验（Chemical principle experiment - distillation synthesis experiment）.docVIP

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化工原理实验——精馏综合实验（Chemical principle experiment - distillation synthesis experiment）.doc

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化工原理实验——精馏综合实验（Chemical principle experiment - distillation synthesis experiment）

化工原理实验——精馏综合实验（Chemical principle experiment - distillation synthesis experiment） This article is contributed by bolivia2010 Doc documents may have a poor browsing experience at the WAP end. It is recommended that you choose TXT, or download the source file to the native view. Experiment of eight distillation experiments One, the purpose of the experiment The basic structure of plate distillation column, the process of distillation equipment and the function of various parts. The effects of different reflux ratio on the efficiency of rectification tower are studied. 3. Master the measurement and balance phase diagram of binary system gas liquid. 4. Grasp the use of abbe refractometer 2. Experimental contents Index of refractive index - part I: part I: the calibration of the standard curve of ethanol quality components. Experiment scheme design, require the use of abbe refractometer, respectively different ethanol ─ quality components are the refractive index of propyl alcohol solution. Draw the index of discount - ethanol mass composition standard curve, regression linear formula W = A * nD + B. Among them: W is the mass fraction of ethanol and nD is the index of refractive index. The second part: determination of the balance of gas liquid in binary system (the second part: the relation curve of the relationship between the gas liquid equilibrium (t-x - y) and (x-y) curve of the binary system. Requires the use of two from balance experiment device were determined for different quality components of ethanol ─ is propyl alcohol solution of equilibrium temperature (t), liquid molar group (x), gas phase composition Moore (y). Draw the dienergy balance phase diagram (t-x-y) and x-y. Part 3: the performance measurement of the rectification tower, which determines the total value of the whole tower of the whole tower, and the total plate efficiency. ET = NT x 100% NP Xn? 1? Xn * xn? 1? xn Among them: NP is the actual plate number of plate rectification tower. 2. Determinat