生产中及实验中英语表达.pdf

STANDARDIZED PHRASE FOR REPORT/报告标准用语 Process Description/工艺描述 No. Unit Operations Process description in Chinese Process description in English 装有机械搅拌(或磁力搅拌)，加料漏斗，温度计(或分 A 3L three-necked round bottom flask equipped with mechanical stirrer (or magnetic 水器，干燥管)的3L 三口瓶 stirrer), addition funnel and thermometer (or Dean-Stock; drying tube) 反应中所用的所有瓶子，真空条件下加热30min，氮 All flasks used in the reaction were heated under vacuum for 30 minutes and purged 气吹扫10min。 with nitrogen for 10 minutes. Instrument/Equipment A 500L autoclave reactor was filled with nitrogen to increase the pressure to 将500L 高压釜通氮气至0.4~0.5MPa 。若0.5~1h 内 1 preparation 0.4~0.5MPa. If the pressure had no change within 0.5~1h, then the air-tightness of the 压力无变化，则气密性良好。 仪器/设备准备 autoclave reactor was good. 将500L 搪瓷釜抽真空到-0.08MPa，再通氮气至常 A 500L glass-lined reactor was evacuated to less than -0.08MPa, then filled with 压。重复进行3 次。 nitrogen to normal pressure. This was repeated for 3 times. o o 将1000L 钛钢釜于60 C用氮气烘6~8h，然后降温 A 1000L titanium reactor was dried at 60 Cwith hot nitrogen for 6~8h, then cooled to 到20~25oC。