两种离子液体双水相体系萃取葛根素的比较（The comparison of the extraction of puerarin from two ionic liquid double water systems）.doc

两种离子液体双水相体系萃取葛根素的比较（The comparison of the extraction of puerarin from two ionic liquid double water systems） The comparison of the extraction of puerarin from two ionic liquid double water systems Author: cao jing, fan jieping, kong tao, zhang lu [abstract] objective: to establish [Bmim] BF4 / NH4) 2S04 and [Braim] BF4 / NaH2P04 two types based on room temperature Ion liquid/salt water phase extraction system is used for extraction and separation of puerarin. Method pair The two systems are optimized to investigate the amount of ionic liquid, the amount of salt and the amount of puerarin The effect of different alcohols on the distribution of puerarin in two phases. The results were optimized by optimizing the experimental conditions Under the favorable conditions: (NH4) 2S04 dosage is 0.3? 0.36 g/ml, [Bmim] BF4 is 0.32? 0.40 g/ml, puerarin solution was 1.5 ml, ethanol was 2%, and the extraction rate of puerarin was ok More than 97 percent. Conclusion [Bmim] BF4 / (NH4) 2S04 dual water phase system has higher extraction rate for ge root, In addition, the extraction rate of puerarin was significantly increased when a small amount of ethanol was added. [keywords] ion liquid; Double water phase; Puerarin; Extraction separation Abstract: ObjectiveTwo ionic liquids aqueous two - phase systems Based on [Bmim] BF4 / (NH4) 2S04 and [Bmim] BF4 / NaH2P04 were To obtain the effective constituent, puerarin from pueraria. Methods Experimental conditions of each of these two systems were optimized. Including the amount of ionic liquid, salt, puerarin and Alcohol. The Results After optimizing the experimental the conditions, the Best conditions were the amount of (NH4) 2S04 for 0. 0. % g/ral, [Bmim] BF4 for 0.32? 0.40 g/ml, adding 1. 5 ml puerarin solution, The extraction efficiency of puerarin could be up to 97%. ConclusionThe [Bmim] BF4 / (NH4) 2 s04 system has a who extraction Efficiency of puerarin Efficiency can happens evidently. Key words: Ionic liquid; Aqueous two - phase