具有高介电常数特性涂层的选取与试验.docxVIP

具有高介电常数特性涂层的选取与试验摘要：目的为了克服现有铁氟龙涂层介电常数低，使用寿命短等缺点，寻求并制备具有高介电常数且兼有耐磨、耐腐蚀、硬度高，绝缘能力强、化学稳定性好、抗高温氧化能力强等特性的涂层，从而提高探针灵敏度系数及机械性能，提高测量精度，延长使用寿命。方法通过对现有各类涂层的对比，选取Al2O3-3wt%TiO2，Al2O3-13wt%TiO2和Al2O3-20wt%TiO2三种常规粒径的陶瓷粉末进行试验测试，分别评价涂层的绝缘性后优选一种涂层进行喷涂试验、介电常数测试、腐蚀性测试及拉伸测试，并与铁氟龙涂层进行对比。结果 Al2O3-13wt%TiO2和Al2O3-20wt%TiO2两种粉末涂层与基体之间的电阻值分别为0.57MΩ和0.42MΩ，Al2O3-3wt%TiO2陶瓷涂层的绝缘性良好。Al2O3-3wt%TiO2粉末的粒径范围为15-45μm，粒度分布较为分散，该涂层的相对介电常数高达290，是铁氟龙涂层的132倍，涂层表面较为均匀，但存在少量孔隙。经过腐蚀性测试，铁氟龙涂层试样失重为23.4mg，Al2O3-3wt%TiO2涂层试样失重极少，仅为0.40mg，拉伸测试时，当载荷为52KN，试样被拉长20mm时，试样涂层才出现裂缝，而铁氟龙涂层被拉伸7mm时就完全剥落。结论 Al2O3-3wt%TiO2陶瓷涂层绝缘性良好，介电常数相对于铁氟龙涂层提高132倍，粒度的分散性分布能使得喷涂效果更佳，涂层与机体的剪切结合强度高，耐蚀性较强，实验结果表明能够完全替代现有的铁氟龙涂层。关键词：介电常数；涂层；氧化铝；氧化钛；喷涂；腐蚀中图分类号：TE35文献标识码：A?Selection and Experiment forCoating with High Dielectric?ConstantYANG Bo1 ,LI Jie1 ,LI He1(Shaanxi Yanchang Petroleum Company Institute，Xi’an710075)ABSTRACT:ObjectiveIn order to overcome the?low dielectric constant and short life of?existing teflon coating?，seeking and preparation for high dielectric constant ,high wear resistance, good corrosion resistance, hardness, insulating ability, good chemical stability and strong features of high temperature oxidation resistance coating to improve the probe sensitivity coefficient and mechanical performance,as well as the measurement precision.Methods This paper select the three size ofpowder like Al2O3-3wt%TiO2, Al2O3-13wt%TiO2 and Al2O3-20wt%TiO2through comparing the existing various types of coating,respectively evaluate the insulativity .Making a comparison with teflon coating?on the dielectric constant, corrosion test and tensile testafter spraying.ResultsThe resistance value ofAl2O3-13wt%TiO2 and Al2O3-20wt%TiO2 between the coating and the substrate was respectively0.57MΩand 0.42ΩM,andtheAl2O3-3wt%TiO2coating of insulativitywas good. The particle size of Al2O3-3 wt % TiO2 powder was in the range of 15 to 45 microns, and the particle size distribution was dispersed .The relative dielectric constant was 132 times of teflon coating