硫酸亚铁铵的制备及纯度检验（Preparation and purity test of ammonium ferrous sulfate）.docVIP

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2017-08-18 发布于河南
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硫酸亚铁铵的制备及纯度检验（Preparation and purity test of ammonium ferrous sulfate）.doc

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硫酸亚铁铵的制备及纯度检验（Preparation and purity test of ammonium ferrous sulfate）

硫酸亚铁铵的制备及纯度检验（Preparation and purity test of ammonium ferrous sulfate） Preparation and purity test of ammonium ferrous sulfate I. teaching requirements 1. to understand the general characteristics of salt 2. learning complex (NH4) method for preparation of 2SO4 - FeSO4 - 6H2O. 3. familiar with basic inorganic preparation operations such as water bath heating, filtration, evaporation and crystallization. 4. learn the purity of the product. 5.. Understand the quality grade of products by visual inspection Two, preview content 1, commonly used glass (porcelain) instrument: HYPERLINK, javascript:void (null); beaker, triangle bottle, HYPERLINK, javascript:void (null), evaporating dish, Brinell funnel and other methods of use; 2, HYPERLINK, javascript:void (null), pure water for laboratory use and anaerobic water for inspection; 3, prepare some inorganic preparation of basic operations: water bath heating, evaporation, concentration, crystallization, decompression, filtration and so on; 4, HYPERLINK, javascript:void (null); check the solubility data table of the substance; HYPERLINK javascript:void (null); the influence of temperature on solubility; The nature of the 5, salt, (NH4) the preparation method of 2SO4 - FeSO4 - 6H2O; 6, (NH4) 2SO4. FeSO4. 6H2O purity test method; 7. Learn how to inspect the quality grades of products by visual colorimetry. Three 、 experimental principle Ammonium ferrous sulfate (NH4) 2SO4 - FeSO4 - 6H2O) brand name Moore salt, as the blue green monoclinic crystal. General ferrous salt is easily oxidized in air, and the ammonium ferrous sulfate in the air than ferrous salt should be stable, not easy to be oxidized, and the price is low, the manufacturing process is simple, easy to get the pure crystal, so it is widely used. In quantitative analysis, a standard solution used to prepare ferrous ions (think 1). Like other salt, (NH4) 2SO4 - FeSO4 - 6H2O solubility in water than the composition of each of its component FeSO4 or (NH4) the solubility