植物性样品中农药残留多色谱质谱筛选和确证体系的研究.PDF

4 1 Vol. 4 No. 1 2013 2 Journal of Food Safety and Quality Feb. , 2013 卢大胜, 徐 骞, 陈 冲, 冯 超, 林元杰, 金玉娥, 熊丽蓓, 汪国权* ( , 200336) 摘 要 : 目的 , GPC-GC-MS LC-QToF GC-MS/MS , 方法 FAPAS , (d-SPE) , GPC-GC-MS LC-QToF , , , GC-MS/MS 结果 GPC-GC-MS LC-QToF 4 , GC-MS/MS , FAPAS , Z 0.5 结论 3 关键词: ; ; GPC-GCMS; LC-QToF; GC-MS/MS Screening and confirmation of non-target pesticide residues in plant samples using a combined system of GPC-GC-MS, LC-ToF and GC-MS/MS LU Da-Sheng, XU Qian, CHEN Chong, FENG Chao, LIN Yuan-Jie, JIN Yu-E, * XIONG Li-Bei, WANG Guo-Quan (Shanghai Municipal Center for Disease Control and Prevention, Shanghai 200336, China) ABSTRACT: Objective To establish a method for the screening and confirmation of non-target pesticides in plant samples based on the techniques of gel permeation chromatography-gas chromatography-mass spec- trometry (GPC-GC-MS) and liquid chromatography-quaqrupole-time of flight mass spectrometry (LC-QToF). Methods After a sample pretreatment including extraction with acetic acid/acetonitrile buffer system follow- ing water immersion, cleaning up with dispersive solid-phase extraction and concentration, the sample was separately analysed