carbon nano material synthesis from polyethylene by chemical vapour deposition从聚乙烯碳纳米材料合成化学蒸汽沉积.pdfVIP
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carbon nano material synthesis from polyethylene by chemical vapour deposition从聚乙烯碳纳米材料合成化学蒸汽沉积
Advances in Materials Physics and Chemistry, 2012, 2, 1-10
/10.4236/ampc.2012.21001 Published Online March 2012 (http ://www.SciRP.org/journal/ampc)
Carbon Nano Material Synthesis from Polyethylene by
Chemical Vapour Deposition
1 2 3 1 2*
Pravin Jagdale , Madhuri Sharon , Golap Kalita , Noor Mahmad Nabi Maldar , Maheshwar Sharon
1Chemistry Department, Solapur University, Solapur, India
2N. Shankaran Nair Research Centre for Nanotechnology and Bionanotechnology,
S.I.C.E.S. College, Ambarnath, India
3Department of Electrical Engineering, Chubu University, Kasugai, Japan
* *
Email: sharonmaheshwar@, sharon@iitb.ac.in
Received August 14, 2011; revised October 8, 2011; accepted November 14, 2011
ABSTRACT
Three different types of Polyethylene family, High Density Polyethylene, (HDPE), Low Density polyethylene (LDPE)
and Linear Low Density polyethylene (LLDPE) polymers having different molecular weight and density; were pyro-
lyzed in the temperature range of 550˚C - 1050˚C under H , N and Ar gases. Taguchi Optimization technique was ap-
2 2
plied to find out the best operating conditions to get maximum yield of carbon nano material (CNM). For Taguchi op-
timization, experimental set up was done in two different temperature ranges i.e. 550˚C - 750˚C and 850˚C - 1050˚C.
CNMs synthesized were characterized by SEM, TEM, Micro Raman and XRD analysis. HDPE was found to yield
max
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