formation of coal2o4 nanoparticles via low-temperature solid-state reaction of fine gibbsite and cobalt precursorcoal2o4形成纳米颗粒通过低温固态反应的三水铝矿和钴前驱.pdfVIP

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formation of coal2o4 nanoparticles via low-temperature solid-state reaction of fine gibbsite and cobalt precursorcoal2o4形成纳米颗粒通过低温固态反应的三水铝矿和钴前驱.pdf

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formation of coal2o4 nanoparticles via low-temperature solid-state reaction of fine gibbsite and cobalt precursorcoal2o4形成纳米颗粒通过低温固态反应的三水铝矿和钴前驱

Hindawi Publishing Corporation Journal of Nanomaterials Volume 2012, Article ID 108369, 8 pages doi:10.1155/2012/108369 Research Article Formation of CoAl2O4 Nanoparticles via Low-Temperature Solid-State Reaction of Fine Gibbsite and Cobalt Precursor Natpakan Srisawad,1 Wasu Chaitree,1 Okorn Mekasuwandumrong,2 Piyasan Praserthdam,1 and Joongjai Panpranot1 1 Department of Chemical Engineering, Faculty of Engineering, Center of Excellence on Catalysis and Catalytic Reaction Engineering, Chulalongkorn University, Bangkok 10330, Thailand 2 Department of Chemical Engineering, Faculty of Engineering and Industrial Technology, Silpakorn University, Nakhon Pathom 73000, Thailand Correspondence should be addressed to Joongjai Panpranot, joongjai.p@chula.ac.th Received 13 July 2012; Revised 14 August 2012; Accepted 16 August 2012 Academic Editor: Alireza Khataee Copyright © 2012 Natpakan Srisawad et al. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. Nanocrystalline cobalt aluminate (CoAl O ) was synthesized by the solid-state reaction method with cobalt chloride hexahydrate 2 4 (CoCl ·6H O) as the source of Co and gibbsite (Al(OH) ) as the source of Al, respectively. The eﬀects of particle size of the starting 2 2 3 ﬁne gibbsite (0.6 and 13 μm) and calcination temperatures (450, 550, and 650◦C) on the properties of CoAl O were investigated 2 4