characterization of chemical constituents of luffa operculata(cucurbitaceae)描述化学成分的丝瓜operculata(葫芦科).pdfVIP

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characterization of chemical constituents of luffa operculata(cucurbitaceae)描述化学成分的丝瓜operculata(葫芦科).pdf

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characterization of chemical constituents of luffa operculata(cucurbitaceae)描述化学成分的丝瓜operculata(葫芦科)

American Journal of Analytical Chemistry , 2011, 2, 989-995 doi:10.4236/ajac.2011.28116 Published Online December 2011 (http://www.SciRP.org/journal/ajac) Characterization of Chemical Constituents of Luffa operculata (Cucurbitaceae) 1,3 1 2 Cléia Rocha de Sousa Feitosa , Robério Costa da Silva , Raimundo Braz-Filho , Jane Eire Silva Alencar de Menezes4 5 1 , Sônia Maria Costa Siqueira , Francisco José Queiroz Monte 1 Programa de Pós-Graduação em Química-DQOI-CC, Universidade Federal do Ceará, Fortaleza, Brazil 2 Universidade Estadual do Norte Fluminense Darcy Ribeiro, Campos dos Goytacazes, Brazil 3 Universidade Estadual do Ceará, Faculdades de Educação de Crateús, Fortaleza, Brazil 4 Universidade Estadual do Ceará, Itapipoca Fortaleza , Brazil 5 Universidade Estadual do Ceará, e campos do Itaperi, Fortaleza, Brazil E-mail : fmonte@dqoi.ufc.br Received August 4, 2011; revised September 15, 2011; accepted September 28, 2011 Abstract A mixture of new ceramides (1, 2, 3, 4 and 5) together with a binary mixture of ceramides with long chain alkyl (6 and 7), triterpenoid (10) and steroids (11 and 12) have been isolated from bark of the fruits and of the stems of Luffa operculata (Cucurbitaceae). The structures were elucidated by comprehensive spectro- scopic analysis including 1H and 13C NMR, DEPT (distortionless enhancement by polarization transfer), COSY (correlated spectro