chemical reaction and crystalline procedure of bismuth titanate nanoparticles derived by metalorganic decomposition technique钛酸铋纳米粒子的化学反应和结晶过程导出了摘要分解技术.pdfVIP

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chemical reaction and crystalline procedure of bismuth titanate nanoparticles derived by metalorganic decomposition technique钛酸铋纳米粒子的化学反应和结晶过程导出了摘要分解技术.pdf

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chemical reaction and crystalline procedure of bismuth titanate nanoparticles derived by metalorganic decomposition technique钛酸铋纳米粒子的化学反应和结晶过程导出了摘要分解技术

Materials Sciences and Applications, 2010, 1, 91-96 doi:10.4236/msa.2010.12016 Published Online June 2010 (http://www.SciRP.org/journal/msa) Chemical Reaction and Crystalline Procedure of Bismuth Titanate Nanoparticles Derived by Metalorganic Decomposition Technique 1* 2 1 1 1 1 Weiliang Liu , Xinqiang Wang , Dong Tian , Chenglong Xiao , Zengjiang Wei , Shouhua Chen 1Provincial Key Laboratory of Glass and Ceramics, School of Materials Science and Engineering, Shandong Institute of Light Indus- try, Jinan, China; 2State Key Laboratory of Crystal Materials, Shandong University, Jinan, China. Email: wlliu@; liuwl@ Received February 25th, 2010; revised April 24th, 2010; accepted April 27th, 2010. ABSTRACT The homogeneous bismuth titanate single-phase nanoscaled ceramic powders have been prepared by means of meta- lorganic decomposition. The thermal decomposition/oxidation of the pre-heated precursor, as investigated by differential thermalgravimetric analysis, X-ray powder diffraction, and environment scanning electron microscope, lead to the formation of a well-defined orthorhombic bismuth titanate co mpound. Formation of the layered perovskite-like bismuth titanate occurs via intermediates with sequential changes in the coordination polyhedron of bismuth. The chemical reactions of precursor powder in heat treatment process have been investigated further by Raman and Fourier transform infrared spectra, and the reaction mechanism was tentatively proposed thereafter. Keywords : Reaction Mechanism, Metalorganic Decomposition, Bismuth Titanate, Nanopowders 1. Introduction advantages of low calcining temperature, simplifying