原创力文档effect of nanodisperse carbon fillers and isocyanate chain extender on structure and properties of poly(ethylene terephthalate)nanodisperse碳填充剂和异氰酸酯链extender对结构和性能的聚(乙烯对苯二甲酸乙二醇酯).pdfVIP
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effect of nanodisperse carbon fillers and isocyanate chain extender on structure and properties of poly(ethylene terephthalate)nanodisperse碳填充剂和异氰酸酯链extender对结构和性能的聚(乙烯对苯二甲酸乙二醇酯)
Hindawi Publishing Corporation
Journal of Nanomaterials
Volume 2012, Article ID 870307, 7 pages
doi:10.1155/2012/870307
Research Article
Effect of Nanodisperse Carbon Fillers and
Isocyanate Chain Extender on Structure and
Properties of Poly(ethylene terephthalate)
Vladimir Agabekov,1 Vera Golubovich,2 and Stepan Pesetskii2
1 Institute of Chemistry of New Materials, National Academy of Sciences of Belarus, 36 F. Skoriny Street, 220141 Minsk, Belarus
2 V.A. Bely Metal-Polymer Research Institute, National Academy of Sciences of Belarus, 32a Kirov Street, 246050 Gomel, Belarus
Correspondence should be addressed to Vladimir Agabekov, agabekov@ichnm.basnet.by
Received 10 November 2011; Accepted 29 December 2011
Academic Editor: Sevan P. Davtyan
Copyright © 2012 Vladimir Agabekov et al. This is an open access article distributed under the Creative Commons Attribution
License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly
cited.
The effect of diisocyanate chain extender (CE) on the mechanical, rheological, and relaxation properties, as well as on molecular
weight and crystallizability, of starting poly(ethylene terephthalate) (PET) and its composites containing carbon nanomaterials
(CNM) such as carbon nanotubes (CNTs) and commercial carbon (CC) has been studied. The composites were compounded
in molten PET using twin-screw extruder (screw diameter 35 mm; L/ D = 40). To improve the distribution of CNM in the
polymeric matrix (before introduction into the melt), they were blended with PET powder and subjected to an ultrasonic
treatment in methylene chloride. The salient features of the materials structure were estimated based on DSC and relaxation
spectrometry (dynamic mec
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