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effects of cross linking on the chromatographic nitrogen isotope separation交联对色谱氮同位素分离
American Journal of Analytical Chemistry , 2011, 2, 104-108
doi:10.4236/ajac.2011.22011 Published Online May 2011 (http://www.SciRP.org/journal/ajac)
Effects of Cross Linking on the Chromatographic Nitrogen
Isotope Separation
1 1* 2 2 2
Xunyue Liu , Xingcheng Ding , Tatsuya Suzuki , Masao Nomura , Yasuhiko Fujii
1
Institute of Nuclear Agricultural Science, Zhejiang University, Hangzhou, China
2Research Laboratory for Nuclear Reactors, Tokyo Institute of Technology, Tokyo, Japan
*
E-mail : dingxch@
Received November 15, 2010; revised January 26, 2011; accepted February 9, 2011
Abstract
The effects of cross linking with porous cation exchange resin were studied for nitrogen isotope separation.
The displacement chromatography was conducted by the resin with cross linking rang from 20% to 40%. A
sharp adsorbed ammonium band was maintained for each operation. Enriched 15
N isotopes with 0.93% were
obtained by 20% cross linking resin and two meters chromatographic operation which started from the natu-
ral abundance of ammonium molecule. The effect of cross linking percentage on the height equivalent to a
theoretical plate (HETP) was evaluated in the present work and the HETP value is proportional to the cross
linking percentage. HETP value of 0.036 cm was obtained at the present system by using 20% cross linking
resin.
Keywords: Cross Linking, Chromatography, Nitrogen Isotope, Ion Exchange Resin
1. Introduction
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