超合金奈米晶新制程之研发-YOKE.DOC

718超合金奈米晶與不同等級細晶材料機械性質之比較研究 Comparison of Mechanical Properties among Nanocrystalline and Other Fine Grain Materials of Superalloy 718 侯文星李驊登 王尚智 王偉仁3 黃國禎1 蔡忠君2 W. S. Hou H. T. Lee S. C. Wang W. R. Wang K. C. Huang C. C. Tsai 摘要 晶粒的細化可以大幅提升718超合金機械性質的表現，本研究中探討應用常溫應變加工和後續靜態再結晶處理時，藉由細緻的(相析出及溫度的調整，進行不同晶粒細化等級的控制，首先將材料經高於δ之溫度進行固溶處理，再經充份的冷成形應變及靜態再結晶處理時溫度控制，可以穩定獲得微米晶及次微米晶不同等級之細晶組織，奈米晶製程先材料製成2.5μm細晶材料，再進一步經冷成形及在較低的溫度進行再結晶處理，由本製程獲得200nm之奈米晶，並與其他18μm、 2.5μm細晶、0.75μm超細晶材料進行機械行質的比較，由結果顯示，經時效強化後的奈米晶材料，常溫拉伸展現最高的抗拉強度並具適當的延展性，在650℃應變速率5x10-4s-1的拉伸測試條件下，即顯現超塑性的現象，具最低的高溫抗拉強度和138%極佳的高溫伸長率。 關鍵詞：次微米晶、奈米晶、靜態再結晶和(相 Abstract Grain refinement could improve the mechanical properties of superalloy 718 evidently. The material by solution treated above δ soluvs initially and then follows sufficient cold forming combined with recrystallization treatment. During the recrystallization process by appropriately temperature controlled, a fine and uniformly dispersed δ precipitate to prohibit grain growth and obtain the different grades of microcrystalline and submicrocrystalline structure stably. The nanocrystalline process was study by the initial 2.5μm structure with further cold forming and static recrystallization at lower appropriate temperature. The nanocrystalline with grain size of 200nm was obtained. The mechanical properties of nanocrystalline material were investigated and compare with the other materials with grain size of 18μm, 2.5μm and 0.75μm. According to the test results, nanocrystalline superalloy 718 has the highest ultimate tensile strength (UTS) at room temperature. Due to the superplasticity occur at 650℃, the material have the lowest UTS and 138% superior elongation. Key word: submicrocrystalline, nanocrystalline, static recrystallization and ( phase 1. 前言 晶粒細化材料本來對立的特性指標強度和延展兼，對於718超合金的晶粒細化，已有研究顯示大幅改善強度和低週疲勞等特性(1, 2)，尤其當晶粒細化至10μm以下的等軸晶，在適當的溫度和應變速率下，會有超塑性的展現(2-4)，因此有許多的研究報導細晶材料的製程通常是在熱成型或冷加工之前生成大量的δ相，利用在動態或靜態再結晶時，析出大量δ相，使再結晶過程，阻礙晶界的移動，控制晶粒的成長，而達到晶粒細化