高效液相色谱法测定儿腹康口服液中秦皮甲素及盐酸小檗碱含量文库(Determination of abdominal Er Kang oral liquid of aesculin in Library and the content of Berberine Hydrochloride by HPLC).docVIP
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高效液相色谱法测定儿腹康口服液中秦皮甲素及盐酸小檗碱含量文库(Determination of abdominal Er Kang oral liquid of aesculin in Library and the content of Berberine Hydrochloride by HPLC)
高效液相色谱法测定儿腹康口服液中秦皮甲素及盐酸小檗碱含量文库(Determination of abdominal Er Kang oral liquid of aesculin in Library and the content of Berberine Hydrochloride by HPLC)
Determination of abdominal Er Kang oral liquid in aesculin and berberine.Txt library do not forget once owned by high performance liquid chromatography; not to be cherished; not to give up their own lost memories.
Determination of abdominal Er Kang oral liquid in aesculin and berberine hydrochloride by HPLC
Update Date: 2010-06-08 Click: Wang Haibo, Zhang Yongguang, Sun Bo, Yang Junfeng
Abstract: the determination of abdominal Er Kang oral liquid in aesculin and berberine hydrochloride by HPLC. With eighteen alkyl silane bonded silica as the stationary phase, the mobile phase with gradient elution, 1: methanol: water (27: 73), mobile phase II: acetonitrile: 0.05mol/L twelve sodium dodecyl sulfate solution (54: 46), the detection wavelength of 354nm. The method of sample liquid has the advantages of simple preparation, good reproducibility, the recovery rate of aesculin was 99.75%, berberine hydrochloride was 100.59%.
Keywords: @ children abdominal Kang oral liquid / chemical / chemical; @ aesculin; @ berberine hydrochloride / chemistry; chromatography, high performance liquid chromatography
CLC number: R284.1, document identification code: A, article number: 1003-9783 (1999) 06-0370-02
Fetal abdominal Kang oral liquid is composed of five herbs of Rhizoma Coptidis, Radix Pulsatillae, cortex Fraxini, rice shell, mainly used for infantile viral diarrhea. This paper mainly cortexfraxini a HPLC method in the other main drug and berberine hydrochloride were determined. The method is simple, practical, report as follows now.
1 materials and methods
1.1 instrument and reagent Waters600 high performance liquid chromatography; Waters486 UV detector; PC800 platform.
Aesculin (740-9403), berberine hydrochloride (713-9304) control products are provided by China control of pharmaceutical and biological products. Acetonitrile is c
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