凝固点降低法测定摩尔质量思考题（Determination of molar mass by freezing point depression method）.docVIP

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凝固点降低法测定摩尔质量思考题（Determination of molar mass by freezing point depression method）.doc

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凝固点降低法测定摩尔质量思考题（Determination of molar mass by freezing point depression method）

凝固点降低法测定摩尔质量思考题（Determination of molar mass by freezing point depression method） Determination of molar mass by freezing point reduction method 1, in order to improve the accuracy of the experiment, is it possible to increase the value of the solute concentration method? Answer: No, too much solute, not a dilute solution, does not agree with the freezing point. 2, ice bath temperature is too high or too low, what is wrong? Answer: too high will lead to too slow cooling, too low can not determine the correct freezing point. 3, mixing speed too fast and too slow, whats the impact on the experiment? Answer: in the process of gradually decreasing temperature, stirring too fast, not too cold, stirring too slowly, the system temperature is uneven. When the temperature picks up, the stir is too fast, the highest point of recovery is due to the heat of mixing, and the sound is too high; too slow, the freezing point of the solution is low. Therefore, the role of mixing is to make the system temperature uniform, and the two is heating (especially scraping the wall), to promote the formation of new solid phase. 4, according to what principle, considering the amount of added solute, too much or too little will have an impact? Answer: according to the number of dilute solution, the amount of solute added is small, but for weighing relative precision, the solute can not be too little. 5, freezing point method to determine molar mass, how about the range of use? Answer: dilute solution 6, the freezing point drops according to what phase equilibrium system and what kind of phase line Answer: the melting point of the two component eutectic system, also known as the saturation line of a substance 7. Why use an air cannula instead of its effect on the experimental results? Answer: slow down the rate of cooling to prevent over approval. 8 if the solute has dissociation in solution, what is the effect on the determination of molar mass? Answer: as the freezing point drops, how much dire