土壤有机质含量测定（Soil organic matter content determination）.docVIP

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土壤有机质含量测定（Soil organic matter content determination）.doc

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土壤有机质含量测定（Soil organic matter content determination）

土壤有机质含量测定（Soil organic matter content determination） DOC documents may experience poor browsing on the WAP side. It is recommended that you first select TXT, or download the source file to the local view. Determination of soil organic matter Potassium dichromate volumetric method -- external heating method, potassium dichromate volumetric method -- external heating method The 1 Principle: principle with quantitative potassium dichromate sulfuric acid solution, in the electric heating conditions, the oxidation of organic matter in the soil, the residual dichromate with ferrous sulfate standard solution titration, and the actual calibration blank based on silica additives, according to the quality difference between before and after oxidation of oxidant, calculate the amount of organic carbon, multiplied by the coefficient 1.724, the content of soil organic matter. Equipment: 2 equipment: 1/10000 analytical balance; electric bath (Shi Layu); test tube; neck funnel; flask set clock; burette: 5.00ml; thermometer: 200 to 300 DEG C; wire screen: aperture 0.25mm 3 reagent; unless otherwise specified, the reagents used were of pure. 3.1 silver sulfate: Inquiry into powder; 3.2 silica powder; 3.3 phenanthroline indicator: Taking o - Phenanthroline 1.490g dissolved in 100ml aqueous solution containing 0.700g of ferrous sulfate, this indicator is easy to deteriorate, should be sealed and stored in brown flasks; 3.4 0.4mol - L (1/6 - K2Cr2O7 potassium dichromate) sulfuric acid solution: weigh 40.0g of potassium dichromate, dissolved in 600 ~ 800ml -1 Distilled water, after being completely dissolved and diluted with water to 1L, the 3L solution into a beaker; another 1L proportion of 1.84 concentrated sulfuric acid, slowly pour potassium dichromate in aqueous solution, stirring constantly, in order to avoid the sharp warming, each about 100ml sulfuric acid after the pause, and the burning cup of cold water in the Sheng basin cooling, the temperature of the solution to be reduce