土壤全氮测定方法3（Soil total nitrogen determination method 3）.docVIP

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土壤全氮测定方法3（Soil total nitrogen determination method 3）.doc

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土壤全氮测定方法3（Soil total nitrogen determination method 3）

土壤全氮测定方法3（Soil total nitrogen determination method 3） This article is contributed by obeilia DOC documents may experience poor browsing on the WAP side. It is recommended that you first select TXT, or download the source file to the local view. Soil total nitrogen method (half trace method) half trace Kjeldahl method Principle: 1 Principle: the sample in the acceleration agent participation, with concentrated sulfuric acid when cooking, all kinds of organic compounds containing nitrogen, through the complex high temperature decomposition reaction, into ammonium nitrogen. The ammonia distilled after alkalization is absorbed by boric acid, and the total nitrogen content of the soil (excluding all nitrate nitrogen) is determined by acid standard solution. Total nitrogen, including nitrate and nitrite nitrogen, was determined before the sample was removed. First the nitrite nitrogen oxidation in samples of nitrate nitrogen by Potassium Permanganate, with all the reduction of iron nitrate reduction, converted to ammonium nitrogen. Equipment: 2 equipment: crusher screen: 1/10000 soil samples; soil analysis balance; B CHI B-339 Automatic Kjeldahl nitrogen determination apparatus and digestion equipment; 3 reagent 3.1 sulfuric acid or hydrochloric acid: pure 0.005mol L -1 analysis, 0.01 mol - L -1 sulfuric acid or hydrochloric acid standard solution 3.2: industrial sodium hydroxide; or chemically pure, 10 mol - L -1 3.3 sodium hydroxide solution; accelerating agent: 100g potassium sulfate (Hua Xuechun), 10g (five copper sulfate hydrate chemical pure 1g powder and mortar), in fine, must be mixed evenly. 3.45% Potassium Permanganate 25g Potassium Permanganate 500ml solution: dissolved in deionized water and stored in a brown bottle; 3.5 1:1 sulfuric acid; 3.6 iron powder: ground through the aperture 0.15mm (100 mesh sieve; 3.7 octanol). Determination of 4. step 4.1 soil sample digestion digestion 4.1.1 does not include nitrate and nitrite nitrogen: weigh the air dried soil (t