HAAKE转矩流变仪在高分子材料中的应用.ppt

美国热电集团: 简介 24亿美金 年销售收入 2 reporting segments, 6 大部门 超过10,000员工 在全球30个国家开展业务 Headquarter near Boston, MA Thermo Karlsruhe, German Facility热电集团卡斯鲁贺 德国工厂（原HAAKE哈克公司） 13.200 m2 230 Employees Fully integrated sheet metal, paint, prefab and wire harness capabilities Cellular manufacturing Product engineering Compliance and regulatory engineering - can provide “consulting” Sales, marketing, service, finance Your partner for Material Characterization (MC) Your Partner for the Laboratory (MC) Your Partner for the Process and Production (MC) Material Characterization – Process and Production 橡胶配方设计 聚合物在液体状态下进行加工 : (挤出、注射) 流动性（粘度）会影响 加工过程 和最终产品的质量: 转矩流变仪是按比例缩小的生产设备 (密炼机、挤出机、口模、辅机设备) 测试过程模拟生产 RheoDrive主机 + 混合器/挤出机 测试器 = PolyLab OS PolyLab OS 转矩流变仪– New Design PolyLab OS 转矩流变仪– New Design Change from Mixer to Extruder Laboratory Mixersmeasuring principle Rotors for Rheomix mixers 混合器所用的转子 Mixer Test PolyView Routine evaluationCurve Type 1 曲线类型1 Materials: Polyolefins:(Polyethylene PE  Polypropene PP ) Engineering Plastics: (PS, PA, PC, PEEK, LCP ) Point detection: L = Loading point 加料峰 M = Minimum point 最低点 PolyView Routine EvaluationCurve type 1 Loading Point 加料峰 Detects complete mixer loading. Point is only used as time base for further calculations Torque value depends on the loading conditions 可得知物料的完全加入，加料峰只作为进一步计算的时间基点，转矩值和加料情况有关。 Minimum point可得到最低熔体粘度 PolyView Routine evaluationCurve Type 2 曲线类型2 Materials: PVC (rigid) Point detection: L = Loading point 加料峰 V = Valley point 谷点(starting point of melting process 熔融过程的起始点) F = Fusion point 熔点 ( melting process finished 熔融过程结束) M = Minimum point PolyView Routine evaluationCurve Type 2 Loading Peak:可得知物料的完全加入，加料峰只作为进一步计算的时间基点，转矩值和加料情况有关，受到加料速度和加料负载的影响。 Valley Point:显示PVC干粉开始熔融，此点对配方设计非常重要 Fusion Peak:显示PVC干粉熔融结束，此点对配方设计非常重要.由于摩擦生热，从此点开始，转矩逐渐降低 Minimum Point:显示熔体粘度达到最低的时间 PolyView Routine evaluationCurve Type 3 曲线类型3 Materials: PVC (rigid) Stability test PVC