原创力文档polymerization of cyclic esters initiated by carnitine and tin (ii) octoate聚合环酯碱和锡(ii)发起辛酸酯.pdf
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polymerization of cyclic esters initiated by carnitine and tin (ii) octoate聚合环酯碱和锡(ii)发起辛酸酯
Molecules 2009, 14, 621-632; doi:10.3390/molecule
OPEN ACCESS
molecules
ISSN 1420-3049
/journal/molecules
Communication
Polymerization of Cyclic Esters Initiated by Carnitine and Tin
(II) Octoate
Marcin Sobczak * and Waclaw Kolodziejski
Department of Inorganic and Analytical Chemistry, Faculty of Pharmacy, Medical University of
Warsaw, ul. Banacha 1, 02-097 Warsaw, Poland; E-mail: waclaw@.pl (W. K.)
* Author to whom correspondence should be addressed; E-mail: marcin.sobczak@.pl (M. S.);
Tel.: +48 22 572 07 55; Fax: +48 22 572 07 84.
Received: 20 October 2008; in revised form: 4 January 2009 / Accepted: 6 January 2009 / Published:
4 February 2009
Abstract: Low-molecular weight poly(ε-caprolactone), polylactides and copolymers of
ε-caprolactone and lactides were obtained by the polymerization of cyclic esters in the
presence of a carnitine/SnOct2 system. Their structures were proven by means of
MALDI-TOF, IR and NMR studies. Effects of temperature, reaction time and carnitine
dosage on the polymerization process were examined.
Keywords: Carnitine; Biomaterials; Polycaprolactone; Polylactide; Ring-opening
polymerization.
Introduction
Pharmacy and medicine are among the most important application fields of polymers. Polymers are
used in production of prosthetic and dental materials, artificial organs, sutures and disposable hygiene
products, active macromolecular pharmaceutical substances, blood substitutes, auxiliary materials and
excipi
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