原创力文档preparation and characteristics of siox coated carbon nanotubes with high surface areasiox涂层的制备、特点与高表面积碳纳米管.pdfVIP
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preparation and characteristics of siox coated carbon nanotubes with high surface areasiox涂层的制备、特点与高表面积碳纳米管
Nanomaterials 2012, 2, 206-216; doi:10.3390/nano2020206
OPEN ACCESS
nanomaterials
ISSN 2079-4991
/journal/nanomaterials
Article
Preparation and Characteristics of SiOx Coated Carbon
Nanotubes with High Surface Area
Aeran Kim 1,2, Seongyop Lim 1,2,*, Dong-Hyun Peck 1, Sang-Kyung Kim 1,2, Byungrok Lee 1 and
Doohwan Jung 1,2
1 Fuel Cell Research Center, Korea Institute of Energy Research, Daejeon 305-343, Korea;
E-Mails: aeran6608@ (A.K.); dhpeck@kier.re.kr (D.-H.P.); ksk@kier.re.kr (S.-K.K.);
brlee@kier.re.kr (B.L.); doohwan@kier.re.kr (D.J.)
2 Advanced Energy Technology, University of Science Technology, Daejeon 305-350, Korea
* Author to whom correspondence should be addressed; E-Mail: sylim@kier.re.kr;
Tel.: +82-42-860-3073; Fax: +82-42-860-3739.
Received: 2 May 2012; in revised form: 8 June 2012 / Accepted: 11 June 2012 /
Published: 18 June 2012
Abstract: An easy method to synthesize SiO coated carbon nanotubes (SiO -CNT)
x x
through thermal decomposition of polycarbomethylsilane adsorbed on the surface of CNTs
is reported. Physical properties of SiO -CNT samples depending on various Si contents and
x
synthesis conditions are examined by X-ray diffraction (XRD), X-ray photoelectron
spectroscopy (XPS), nitrogen isotherm, scanning electron microscope (SEM), and
transmission electron microscope (TEM). Morphology of the SiO
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