原创力文档syntheses of (diacetoxyiodo)arenes or iodylarenes from iodoarenes, with sodium periodate as the oxidant(diacetoxyiodo)芳烃的合成或从iodoarenes iodylarenes,以高碘酸钠为氧化剂.pdfVIP
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syntheses of (diacetoxyiodo)arenes or iodylarenes from iodoarenes, with sodium periodate as the oxidant(diacetoxyiodo)芳烃的合成或从iodoarenes iodylarenes,以高碘酸钠为氧化剂
Molecules 2001, 6, 881-891
molecules
ISSN 1420-3049
Syntheses of (Diacetoxyiodo)arenes or Iodylarenes from
Iodoarenes, with Sodium Periodate as the Oxidant†
Pawel Kazmierczak, Lech Skulski* and Lukasz Kraszkiewicz
Chair and Laboratory of Organic Chemistry, Faculty of Pharmacy, Medical University, Banacha 1, PL
02-097 Warsaw, Poland
† This paper was presented at the Fifth Electronic Conference on Synthetic Organic Chemistry
(ECSOC-5), September 1-30, 2001 (Paper A0005).
* Author to whom correspondence should be addressed; Tel/Fax: +48(22)8226843; e-mail:
lskulski@.pl
Received: 27 September 2001; in revised form 11 October 2001 / Accepted: 12 October 2001 /
Published: 31October 2001
Abstract. - Easy, safe, and effective novel methods for preparing either (diacetoxyiodo)-
arenes, ArI(OAc) , or iodylarenes, ArIO , from the corresponding iodoarenes, ArI, using
2 2
sodium periodate as the oxidant are presented in this paper. In order to obtain 2- and 4-
iodylbenzoic acids, the respective sodium salts of 2- and 4-iodobenzoic acids should be
used as the starting substrates, because mixtures containing the corresponding iodosyl
derivatives as the main products along with the intended iodyl compounds are produced
from the free parent acids.
Keywords: (Diacetoxyiodo)arenes, iodylarenes, iodoarenes, sodium periodate as oxidant
Molecules 2001, 6 882
Introduction
(Diacetoxyiodo)arenes,
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