原创力文档synthesis and molecular structure of tert-butyl 4-(2-tert-butoxy-2-oxoethyl)piperazine-1-carboxylate合成和分子结构的叔丁基4 -(2-tert-butoxy-2-oxoethyl)piperazine-1-carboxylate.pdfVIP
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synthesis and molecular structure of tert-butyl 4-(2-tert-butoxy-2-oxoethyl)piperazine-1-carboxylate合成和分子结构的叔丁基4 -(2-tert-butoxy-2-oxoethyl)piperazine-1-carboxylate
Crystals 2012, 2, 90-95; doi:10.3390/cryst2010090
OPEN ACCESS
crystals
ISSN 2073-4352
/journal/crystals
Communication
Synthesis and Molecular Structure of tert-Butyl 4-(2-tert-butoxy-
2-oxoethyl)piperazine-1-carboxylate
Constantin Mamat 1,*, Anke Flemming 2 and Martin Köckerling 2
1 Institut für Radiopharmazie, Helmholtz-Zentrum Dresden-Rossendorf, Bautzner Landstraße 400,
D-01328 Dresden, Germany
2 Institut für Chemie, Anorganische Festkörperchemie, Albert-Einstein-Straße 3a, D-18059 Rostock,
Germany; E-Mail: Martin.Koeckerling@uni-rostock.de (M.K.)
* Author to whom correspondence should be addressed; E-Mail: c.mamat@hzdr.de;
Tel.: +49-351-260-2805; Fax: +49-351-260-3232.
Received: 20 December 2011; in revised form: 30 January 2012 / Accepted: 31 January 2012 /
Published: 6 February 2012
Abstract: The crystal and molecular structure of tert-butyl 4-(2-tert-butoxy-2-oxoethyl)-
piperazine-1-carboxylate is reported. The title compound crystallizes from a petroleum
ether/ethyl acetate mixture in the monoclinic space group P 21/c with four molecules in the
unit cell. The unit cell parameters are: a = 8.4007(2) Å, b = 16.4716(4) Å,
3
c = 12.4876(3) Å; β = 90.948(1)° and V = 1727.71(7) Å . Bond lengths and angles of this
piperazine-carboxylate are typical.
Keywords: piperazines; building blocks; X-ray structure
1. Introduction
The piperazine moiety plays an important role and is foun
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