the crystal and molecular structure of (2z)-2-[3-(4-methoxybenzoyl)-4,4-dimethyl-1,2-oxazolidin-2-ylidene]-1-(4-methoxyphenyl)ethanone的晶体和分子结构(2 z)2 -[3 -(4-methoxybenzoyl)4、4-dimethyl-1 2-oxazolidin-2-ylidene]1 -(4-methoxyphenyl)ethanone.pdfVIP

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the crystal and molecular structure of (2z)-2-[3-(4-methoxybenzoyl)-4,4-dimethyl-1,2-oxazolidin-2-ylidene]-1-(4-methoxyphenyl)ethanone的晶体和分子结构(2 z)2 -[3 -(4-methoxybenzoyl)4、4-dimethyl-1 2-oxazolidin-2-ylidene]1 -(4-methoxyphenyl)ethanone.pdf

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the crystal and molecular structure of (2z)-2-[3-(4-methoxybenzoyl)-4,4-dimethyl-1,2-oxazolidin-2-ylidene]-1-(4-methoxyphenyl)ethanone的晶体和分子结构(2 z)2 -[3 -(4-methoxybenzoyl)4、4-dimethyl-1 2-oxazolidin-2-ylidene]1 -(4-methoxyphenyl)ethanone

Crystals 2011, 1, 229-235; doi:10.3390/cryst1040229 OPEN ACCESS crystals ISSN 2073-4352 /journal/crystals Article The Crystal and Molecular Structure of (2Z)-2-[3-(4- Methoxybenzoyl)-4,4-dimethyl-1,2-oxazolidin-2-ylidene]-1-(4- methoxyphenyl)ethanone Anna Petrov 1, Roderick C. Jones 2, Douglas G. Vaughan 2, Alan J. Lough 3,† and Robert A. Gossage 1,* 1 Department of Chemistry Biology, Ryerson University, 350 Victoria Street, Toronto ON M5B 2K3, Canada 2 Department of Chemistry, Acadia University, Wolfville NS B4P 2R6, Canada 3 Department of Chemistry, University of Toronto, 80 St. George Street, Toronto ON M5S 3H6, Canada; E-Mail: alough@chem.utoronto.ca † Queries concerning specific aspects of the crystal structure determination should be directed to this author. * Author to whom general correspondence should be addressed; E-Mail: gossage@ryerson.ca; Tel.: +1-416-979-5000; Fax: +1-416-979-5044. Received: 14 September 2011; in revised form: 20 October 2011 / Accepted: 28 October 2011 / Published: 31 October 2011 Abstract: The crystal and molecular structure of the title compound, viz., (2Z)-2-[3-(4- methoxybenzoyl)-4,4-dimethyl-1,2,-oxazolidin-2-ylidene]-1-(4-methoxyphenyl)ethanone (4), is reported. Compound 4 crystallises from toluene/hexanes mixtures in the P21/c space group with eight molecules in the unit cell. The unit cell parameters are: a = 20.9410(11) Å, 3 b = 8.7523(5) Å, c = 21.2291(9) Å; β = 93.529(3)°