the preparation and characterization of poly(m-phenylene- isophthalamide) fibers using ionic liquids的制备和表征聚间苯- isophthalamide)纤维使用离子液体.pdfVIP

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the preparation and characterization of poly(m-phenylene- isophthalamide) fibers using ionic liquids的制备和表征聚间苯- isophthalamide)纤维使用离子液体.pdf

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the preparation and characterization of poly(m-phenylene- isophthalamide) fibers using ionic liquids的制备和表征聚间苯- isophthalamide)纤维使用离子液体

Int. J. Mol. Sci. 2007, 8, 680-685 International Journal of Molecular Sciences ISSN 1422-0067 © 2007 by MDPI /ijms Full Research Paper The Preparation and Characterization of Poly(m-phenylene- isophthalamide) Fibers Using Ionic Liquids Tingting Zhao*, Huaping Wang, Yumei Zhang, Biao Wang and Jianming Jiang State Key Laboratory for Modification of Fibers Materials, Donghua University, Shanghai 200051, P. R. China; E-mail: zhaott@; E-mail: wanghp@. E-mail: zhangym@; E-mail: wangb@; E-mail: jiangjm@ * Author to whom correspondence should be addressed; E-mail: zhaott@ Received: 12 March 2007; in revised form: 14 May 2007 / Accepted: 20 June 2007 / Published: 17 July 2007 Abstract: A process to produce fibers from Poly(m-phenyleneisophthalamide)(PMIA) solution in an ionic liquid via wet-spinning technology are described. The spinning process was investigated on a small laboratory scale. Ionic liquid spinning solutions were first prepared for PMIA fibers, followed by wet spinning. In the course of this research, the physical properties of the PMIA fibers were estimated. We studied the dependence of the mechanical properties of the obtained PMIA fibers on the composition of the coagulation bath, and on the choice of solvent in spinning solution. The morphology of the fibers from ionic liquid and traditional DMAc solvents via wet-spinning process were observed by