硅锰合金中硅、磷的测定（Determination of silicon and phosphorus in silicon manganese alloy）.docVIP

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硅锰合金中硅、磷的测定（Determination of silicon and phosphorus in silicon manganese alloy）.doc

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硅锰合金中硅、磷的测定（Determination of silicon and phosphorus in silicon manganese alloy）

硅锰合金中硅、磷的测定（Determination of silicon and phosphorus in silicon manganese alloy） Determination of silicon and phosphorus in silicon manganese alloy.Txt woman in mind: you must have good fun to drink good sleep well. Once exhausted, and other women spend our money, live in our room, sleep our husband, soak our boyfriend, but also beat our baby. Determination of silicon and phosphorus in silicon manganese alloy Determination of silicon and phosphorus in silicon, phosphorus and ferrosilicon (determination of phosphorus by adding anhydrous sodium sulfite solution to eliminate manganese interference) Determination of manganese in ferromanganese, manganese alloys Method one Manganese ingot Method two Determination of manganese in ferromanganese, manganese alloys - ammonium ferrous sulfate volumetric method 2.5.1 method feeds The sample with nitric acid and phosphoric acid to dissolve, and in the presence of phosphate, ammonium nitrate to 200 DEG C, two manganese oxidized into trivalent manganese, N - phenyl anthranilic acid as indicator, using ferrous titration of manganese. This method is suitable for the determination of manganese, silicon manganese, manganese metal materials in high manganese manganese. 2.5.2 reagent required 2.5.2.1 nitric acid: specific gravity 1.42 2.5.2.2 phosphoric acid: specific gravity 1.70 2.5.2.3 ammonium nitrate: solid 2.5.2.4 indicator solution: benzene, ortho ortho benzoic acid 0.2g, sodium carbonate 0.2g, dissolved in 100mL hot water. 2.5.2.5: sulfuric acid (14) 2.5.2.6 standard solution of ammonium ferrous sulfate: 0.05N. Ferrous ammonium sulfate, 20g, dissolved in 1 liters sulfuric acid (5 + 95). Calibration method: learn 0.05N 25mL potassium dichromate standard solution in a 150mL conical flask, 20mL water, sulfuric acid (14) 5mL, 2mL phosphate, indicator solution 2 drops immediately with ammonium ferrous sulfate solution (0.05N) to test by titration, cherry red to bright green is the end point. 0.05N standard solution with potassium dic