有机化学实验试题（Organic chemistry experiment questions）.docVIP

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有机化学实验试题（Organic chemistry experiment questions）.doc

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有机化学实验试题（Organic chemistry experiment questions）

有机化学实验试题（Organic chemistry experiment questions） Organic chemistry experiment questions I. preparation of ethyl acetate Two. Preparation of crude P sulfonic acid Three. Preparation of crude nitrobenzene Three. Preparation of ethyl benzoate Four. Purification of ethyl acetate Five. Preparation of nitroso phenol Six. Synthesis of castor acid Seven. Preparation of crude Cyclohexene Eight. Preparation of anhydrous ether Nine. Preparation of absolute ethanol (99.5%) Ten. Synthesis of benzyl acetone Eleven. Preparation of ortho nitrophenol and p-nitrophenol Twelve. Preparation of crude para amino benzene sulfonic acid Thirteen. Preparation of coarse acetanilide Fourteen. Purification of chloroform Fifteen. Preparation of crude acetylsalicylic acid Sixteen. The crude preparation of ethyl bromide Seventeen. Preparation of ethyl acetate Eighteen. Preparation of sulfonyl chloride Nineteen. Two. Preparation of phenyl acetone Organic chemistry experiment The name ______________ score _________________ Experiment Name: preparation of ethyl acetate I. principle: CH3COOHCH3CH2OH CH3COO CH2CH3H2O Two, the experimental steps: (80 points) 15mL mixture of anhydrous ethanol and concentrated sulfuric acid in the 15mL 250mL three neck flask, then the three neck flask pack a thermometer, a dropping funnel and a glass pipe, the glass pipe has even shaped condenser; a condenser tube is communicated with the flask through the tail pipe, with heating, the temperature rise 110 to start with a mixture of funnels into 17.6mL ethanol and acetic acid at 1200C 17.3mL. Continue to heat up until after 1300C, no more liquid is removed until the product is recycled into the recycle bottle. Three, draw the experimental device diagram (10 points) Four. What are the possible impurities in the products obtained? How should I get rid of it? (10 points) Note: ethyl acetate b.p=77.10C, d=0.901 Organic chemistry experiment questions two The name ______________ score _________________ Experiment Name: preparati