超高效液相色谱-串联质谱法检测食用菌中荧光增白剂 determination of fluorescent whitening agents in edible mushrooms by ultra performance liquid chromatography-tandem mass spectrometry.pdfVIP
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超高效液相色谱-串联质谱法检测食用菌中荧光增白剂 determination of fluorescent whitening agents in edible mushrooms by ultra performance liquid chromatography-tandem mass spectrometry
5 9 Vol. 5 No. 9
2014 9 Journal of Food Safety and Quality Sep. , 2014
-
*
张建莹, 肖 锋, 叶 刚, 岳振峰 , 罗 耀, 邓慧芬
( , 518045)
摘 要: 目的 85(fluorescent brightener VBL, VBL)71(fluorescent
brightener CXT, CXT) 113(blankophor BA, BA)-(ultra performance
liquid chromatography-tandem mass spectrometry, UPLC-MS/MS, )方法 60%-,
75 ℃, , UPLC-MS/MS
, 结果 0.0100~0.500 mg/L , r2 0.990,
, 80.0%~101%, 3.4%~11.9%;
0.100 mg/kg结论 , 85
71 113
关键词: ; -; ;
Determination of fluorescent whitening agents in edible mushrooms by ultra
performance liquid chromatography-tandem mass spectrometry
*
ZHANG Jian-Ying, XIAO Feng, YE Gang, YUE Zhen-Feng , LUO Yao, DENG Hui-Fen
(Food Inspection and Quarantine Center , Shenzhen Entry-Exit Inspection and Quarantine Bureau, Shenzhen Key
Laboratory of Detection Technology RD on Food Safety , Shenzhen 518045, China)
ABSTRACT: Objective To establish an ultra performance liquid chromatography-tandem mass
spectrometry method for the determination of three fluorescent whitening agents (fluorescent brightener VBL,
fluorescent brightener CXT and blankophor BA) in
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