运用气质联用色谱检测数据定量评价香精的香气协调性变化研究.pdfVIP

运用气—质联用色谱检测数据定量评价香精 的香气协调性变化 廖 堑，邓 宇 (南昌卷烟厂技术中心，南昌市京东高新开发区金圣工业科技园，330096) 摘要：为了建立不同批次和贮存过程中香精的香气协调性变化程度的定量评价模式，运用数学方法归 纳香精样品的气相色谱一质谱(GC—MS)检测数据，以标准样品为基准，计算不同批次样品和同一样 品在贮存过程中各挥发性组分的百分含量相对于标样的整体变化值(即样品偏差值)，用以定量描述香 精样品香气组分的整体变化程度。本文在相同的实验条件下对7个同种香精样品经GC．MS检测所得百 分含量数据进行计算并比较样品偏差值，进而考察了样品的香气协调性变化，结果与感官评定基本一致。 关键词：气相色谱一质谱；挥发性组分；样品偏差值；香精；香气协调性 EvaluationoftheVariationofAroma Quantitative Harmony inPerfumwith Data Gas Chromatographic—MassSpectrometry LL～OKUN，DENGYU Centerof 330096，China TechnologyNanchangCigarettFactory，Nanchang Abstract：Toa for aroma evaluationmodelthevariationof in developquantitative per- from weresummed Fum，gaschromatographic-mass：spectrometry(GC-MS)dataperfumSamples upby mathematic onthestandard total involatile interm modeling．Based sample，thechange compoundsexpressed of the betweendifferentbatch andthestandard is，thedeviationof percentage sample sample，that samples， are werethenusedtOdescribethetotal ofaroma inthe this calculated．They change compoundsperfum．In were GC—MSunderthesameconditionsandthedatawereobtai—ned paper，7samplesanalyzedby by the deviationsofthe we the ofaroma in withthe comparing samples，thenexploredchange harmonyperfum resultsassanleasthesense adjugement．