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Synthesis and Applications of CdSe Quantum Dots-材料合成化学课件PPT
Cd(CH3)2 + TOPSe + TOPO CdSe/TOPO Fluorescence of the CdSe with different emission (λex ) 365nm * Synthesis and Applications of CdSe Quantum Dots A quantum dot is a nano-particulate semiconductor, whose excitons are confined in all three spatial dimensions. What are Quantum Dots ? Structure of CdSe Quantum Dots Zinc blende Wurtzite Rock salt 戴全钦. 吉林大学博士学位论文,2007 Nucleation Cooling Solvent: TOPO (300℃) Combining Injecting Solution B: Se + TOP Solution A: Cd(CH3)2 + TOP MIT M.G. Bawendi, et al. J. Am. Chem. Soc. 1993, 115 (19): 8706-8715. Prevent further nucleation Room temperature optical absorption spectra of CdSe nanocrystallites dispersed in hexane and ranging in size from ~1.2 nm to 11.5 nm. M.G. Bawendi, et al. J. Am. Chem. Soc. 1993, 115 (19): 8706-8715. CdO + TOPSe + TOPO + TDPA CdSe Solution (270℃) TDPA+TOPO (300-320℃) CdO Se + TOP Nucleation Dissolving Cooling Injecting Cooling X.G. Peng, et al. J. Am. Chem. Soc, 2001. 123(1): 183-184. CdO + Se/ODE + ODE = CdSe X.G. Peng, et al. Angewandte Chemie-International Edition, 2002, 41(13): 2368-2371. Mixture (300℃) OA+ODE CdO Se+ODE Nucleation Dissolving Heating Injecting Cooling L.J. An, et al. Journal of Physical Chemistry C. 2007, 111: 5661-5666. Versatile two-phase approach to synthesize highly luminescent CdE (E=S, Se, Te) QDs. CdAc2 + Na2SeSO3 CdSe Y.D. Li. Inorganic Chemistry. 2008, 47(11): 5022-5028. NaOH OA C2H5OH+H2O CdAc2·H2O Na2SeSO3 Dissolving By stiring By stiring Autoclave (40-150℃) Nucleation Se O S O O Green Methods Y.D. Li, et al. Inorganic Chemistry. 2008, 47(11): 5022-5028. Q. J. Sun, et al. Nature Photonics. 2007,1, 717. TEM Core–shell structures Photo-luminescence Applications of Quantum Dots LED Solar cell Biological probe Medical Imaging Biochip Laser devices Biological Labeling Drug Screening Martin Green “The emergence of semiconductor nanocrystals as the building blocks of nanotechnology has opened up new ways to utilize them in next
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