热处理工艺对fecocrmocby非晶合金涂层磨损及腐蚀性能的影响-材料学专业论文 word格式.docxVIP

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热处理工艺对fecocrmocby非晶合金涂层磨损及腐蚀性能的影响-材料学专业论文 word格式.docx

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热处理工艺对fecocrmocby非晶合金涂层磨损及腐蚀性能的影响-材料学专业论文 word格式

AbstractInthisdissertation,Fe41Co7Cr15Mo14C15B6Y2amorphousalloy coating,preparedbyHighvelocityoxygen-fuel(HVOF) technology, withhighglass formingabilityandhighstrengthhadbeen investigated. Effectofheattreatmentonwear resistancepropertyandcorrosionresistanceofFe-basedamorphouscoatingweresystematicallystudiedmainlybyemployingthewearmachine,electrochemicalstation,thedifferentialscanningcalorimeter(DSC),X-raydiffraction(XRD)andscanningelectronmicroscope(SEM).Thestructureoffully amorphousalloycoatingisuniform,compactandbedded.DSCcurvesofcoatingwithtwocrystallizationpeaks(Tp1 =698℃,Tp2 =822℃)showthatthecoatinghasexcellentthermalstabilitybecauseofthehighglasstransitiontemperature(Tg=576℃).Whencoatingwasheatedat700℃,therearedifferent phase, such as α-Fe, (Fe,Cr)7C3, Fe23(C,B)6 and Co6Mo6C2. Thecrystallizationfractionofcoatingalmostincreasesfrom95.1%(2h)to99.4%(12h)andthegrainsizeofthecoatingincreasesfrom22nm(2h)to54nm(12h).AccordingtoHardnesscurveofFe41Co7Cr15Mo14C15B6Y2amorphousalloycoating,thehardnessvaluefirstincreasesandthendecreaseswiththeincreasingofheattreatmentholdingtime.Thehardnessvalueofamorphous/nano-crystallinecoatingishigherthanthatofthefullyamorphousalloycoating.Thehardnessvaluereachestohighest(892HV)withtheholdingtimefor6hat700℃.Fromthewearingcurveofcoating,itcanbeseenthatthewearresistanceof thecoatingsteadyincreasewith theincreasing ofholdingtime.Thewearresistance oforiginalamorphouscoatingistheworstamongall.Contrary,atholdingtimefor12h,thewearresistanceofamorphous/nano-crystallinecoatingis thebestbecausethewearextentreaches theminimum(0.6mg).TheFe41Co7Cr15Mo14C15B6Y2amorphousandnano-crystallinealloycoatingexhibitsabrasiveandfatiguemechanism.ThepolarizationcurvesoftheFe44Cr16Mo16C18B6amorphousandnano-crystalline alloycoatingin1.0M HClsolutionshowthatthe corrosionresistanceoforiginalcoating(Ecorr=-424mv，icorr=0.2mA·cm-2)withcorrosionpittingflakespitonsurfaceissuperiortothatofnano-crystallinealloycoating.Thecorrosionresistanceofcoatingholdingfor 1