年产5000吨合成甲醛生产工艺的设计.pdfVIP

年产5000吨合成甲醛生产工艺的设计 摘要：甲醛是一种应用非常广泛的化工原料，未来一段时间我国对甲醛的需求 仍然有一定的缺口。本文结合具体的生产量以及目前的甲醛生产工艺技术发展现 况，综合比较后选择“银催化法”制甲醛的工艺，重点探讨了氧化反应阶段工艺 过程，包括氧化反应器的设计和校核，对反应急冷段和冷却段所需要的换热器进 行了详细的计算和说明，并给出了反应操作过程中的操作要点和注意事项。 说明书中还分析了甲醛的物化性质用来指导甲醛的安全生产和运输，设计的 内容主要包括三个板块：物料衡算和能量衡算、反应器的设计、附属设备的设计。 其中为了保证数据的可靠性，使用了强大的化工模拟软件对工艺过程进行仿真模 拟，运用模拟的数据辅助设备选型。通过模拟得到物能衡算数据，该数据与相关 文献上的参数比较符合，文中给出和蒸发器、过热器、氧化反应器、第一吸收塔、 第二吸收塔详细的衡算数据。重点计算了氧化反应器的相关参数，包括设备材料、 塔径、塔高、壁厚等重要参数。最后提供了车间布置图，设备连接图，反应器装 置图。 关键词：甲醛；氧化反应阶段工艺过程；银催化法；反应器的设计； 物能衡算数据 The design of the annual output of 5000 tons of synthetic formaldehyde production process Abstract ： Formaldehyde is a kind of wide application of chemical raw materials, the future demand for a period of time to formaldehyde in China still has certain gap. Combining with specific production and the present status of development of formaldehyde production technology, comprehensive comparison after select silver catalysis formaldehyde technology, phase oxidation process are discussed mainly, including oxidation reactor design and check against the emergency cooling section and cooling section needed to carried on the detailed calculation of heat exchanger and instructions, and gives the reaction operating hints and points for attention in the process of operation. Also analyzed the formaldehyde in the instructions for physical and chemical properties used to direct the safety in production and transportation of formaldehyde, design content mainly includes three parts: the material balance and energy balance, the reactor design, the accessory equipment design. Among them in order to guarantee the reliability of data, using the powerful chemical process simulation software to simulate the process simulation, using the data from simulation auxiliary equipment selection. Objects can balance data is obtained by simulat