fe25cr35ni系合金高温压缩变形行为研究word格式论文.docx

摘 要本文利用金相技术、SEM、EBSD和TEM 等微观组织分析方法，并通过高温 热模拟压缩试验(变形温度：1050℃、1100℃、1150℃和 1200℃，应变速率: 10-2s-1、10-1s-1、1s-1，变形量：10%、30%、50%)比较系统地研究了固溶淬火态 Fe-25Cr-35Ni系合金的高温压缩变形行为，以及固溶工艺对该合金组织及性能的 影响。(1)固溶工艺研究表明，Fe-25Cr-35Ni 系合金的晶粒随固溶温度的升高和保温 时间的延长而增大。硬度测试结果表明，Fe-25Cr-35Ni 系合金的硬度随固溶温度 的升高和保温时间的延长而降低，其硬度值与小晶粒尺寸的关系基本符合 Hall-Petch 公式。(2)1175℃固溶处理后的 Fe-25Cr-35Ni 系合金的高温压缩试验结果表明，Fe- 25Cr-35Ni 系合金在高温压缩过程中，应力与应变速率之间存在包括变形激活能 和温度的双曲正弦关系，其变形激活能为 655.4kJ/mol。应变速率相同，流变应力 随变形温度的升高而降低；变形温度相同时，流变应力随应变速率的升高而增 大，流变应力表现出明显的动态再结晶特征。可用以下方程来描述压缩变形过程 中流变应力与热变形参数之间的关系：ε = 3.4048×1022[sinh(ασ5)4.73 ]exp(? 6.5538×10 )pRT(3)Fe-25Cr-35Ni 系合金高温压缩试样的微观组织分析结果表明，其动态再结晶的程度随形变温度的升高与应变速率的降低而增大，增加变形量有利于动态再 结晶过程趋于完全。1050℃时压缩变形机制是以动态回复为主的软化机制， 1100°C、1150°C 和 1200℃以上时，变形过程中的主要软化机制为动态再结晶。关键词： Fe-25Cr-35Ni 系合金；高温压缩；流变应力；动态再结晶AbstractThe deformation behavior of the Fe-25Cr-35Ni based superalloy was studied by OM, SEM, TEM and EBSD technique. High temperature compression tests which conducted at deformation temperatures ranging from 1050°C to 1200 °C and strain rates ranging from 10-2 ~ 1 s-1in this thesis had been performed. The effect of solution treatment on the microstructure and property of the Fe-25Cr-35Ni based superalloy were also investigated.It was shown that the grain size of the Fe-25Cr-35Ni based superalloy increases with the increase of the solution temperature and holding time by means of the microstructure observation.It has been concluded from the hardness testing results that the hardness decreases with the increase of solution temperature and holding time for the superalloy. The relationship between the hardness and the small grain size conformed well with the Hall-Petch equation.The results of high temperature compression tests of the Fe-25Cr-35Ni based superalloy show that the stress level of the alloy can be presented by Zener-Hollomon parameter in a hyperbolic sine-type equation with the hot activation energy of 655.4 kJ/mol. The flow stress of strongly influenced by temperature and strain rate durin